in neat (no solvent) stirring of mixt. of Cr complex and excess of amine, treating with 50 percent aq. HOAc after cooling (separation of KSCN), filtration, washing (aq. HOAc), residue ((amine)2H2(Cr(SCN)4(amine)2)2) dissolved in EtOH; crystalisation, air drying;
参考文献
Journal of the Indian Chemical Society, , vol. 73, # 2-3 p. 129 - 131
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反应条件
in neat (no solvent) stirring of mixt. of Cr complex and excess of amine, treating with 50 percent aq. HOAc after cooling (separation of KSCN), filtration, washing (aq. HOAc), residue ((amine)2H2(Cr(SCN)4(amine)2)2) dissolved in EtOH; crystalisation, air drying;
参考文献
Journal of the Indian Chemical Society, , vol. 73, # 2-3 p. 129 - 131
