5-溴-6-甲基-2-甲硫基-1H-嘧啶-4-酮合成路线 （共 8 条）
反应条件
bromine; acetic acid 1 h; Heating;
参考文献
Abdel-Fattah, Abdel-Samei Mahmoud; Negm, Abdalla Mohamed; Gaafar, Alaa Eldein Mustafa
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 72, # 1.4 p. 145 - 156
反应条件
1: 82 percent / sodium hydroxide / H2O / 3 h / Heating 2: 63 percent / Br2 / acetic acid / 20 °C View Scheme
参考文献
Abdel-Fattah, Abdel-Samei Mahmoud; Negm, Abdalla Mohamed; Gaafar, Alaa Eldein Mustafa
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 72, # 1.4 p. 145 - 156
反应条件
sodium ethanolate 1) EtOH, 15 min, reflux, 2) 1 h, reflux; Yield given. Multistep reaction;
参考文献
Abdel-Fattah, Abdel-Samei Mahmoud; Negm, Abdalla Mohamed; Gaafar, Alaa Eldein Mustafa
Phosphorus, Sulfur and Silicon and the Related Elements, 1992 , vol. 72, # 1.4 p. 145 - 156
反应条件
1: aqueous H2SO4 2: POCl3 3: benzene; zinc-powder; aq.-ethanolic NH3 View Scheme
参考文献
Matsukawa; Ohta
Yakugaku Zasshi, 1950 , vol. 70, p. 137
Chem.Abstr., 1950 , p. 5886
反应条件
1: aqueous H2SO4 2: POCl3 View Scheme
参考文献
Yakugaku Zasshi, , vol. 70, p. 137
Chem.Abstr., , p. 5886
反应条件
1: aqueous H2SO4 2: POCl3 3: benzene; zinc-powder; aq.-ethanolic NH3 4: benzene; zinc-powder; aqueous NH3 / Reagens 4: NaCl View Scheme
参考文献
Yakugaku Zasshi, , vol. 70, p. 137
Chem.Abstr., , p. 5886
参考文献
Curd et al.
Journal of the Chemical Society, 1946 , p. 720,726
参考文献
Matsukawa; Ohta
Yakugaku Zasshi, 1950 , vol. 70, p. 137
Chem.Abstr., 1950 , p. 5886
