1-苄基-3-羟基吡啶氯化物合成路线 (共 5 条)
反应条件
in toluene Alkylation; 1 h; Heating;
参考文献
Takeuchi, Yasuo; Abe, Hitoshi; Harayama, Takashi
Chemical and Pharmaceutical Bulletin, 1999 , vol. 47, # 6 p. 905 - 906
反应条件
potassium hydroxide in water; dimethyl sulfoxide T=50°C; ΔH(excit.), ΔS(excit.), activation energy; Rate constantThermodynamic data;
参考文献
Rajasekar, N.; Srinivasan, V. S.; Venkatasubramanian, N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 8 p. 800 - 802
反应条件
1: NaH / methanol / Heating 2: NaBH4 / methanol / 0 °C View Scheme
参考文献
Takeuchi, Yasuo; Abe, Hitoshi; Harayama, Takashi
Chemical and Pharmaceutical Bulletin, 1999 , vol. 47, # 6 p. 905 - 906
反应条件
methanol; rhodium contaminated with carbon Hydrogenation;
参考文献
Shapiro et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 5140,5145
反应条件
1: NaH / methanol / Heating 2: NaBH4 / methanol / 0 °C 3: tetrahydrofuran / 20 °C View Scheme
参考文献
Takeuchi, Yasuo; Abe, Hitoshi; Harayama, Takashi
Chemical and Pharmaceutical Bulletin, 1999 , vol. 47, # 6 p. 905 - 906