1,6-脱水-2,4-O-苯基-Β-D-吡喃葡萄糖合成路线 （共 12 条）
反应条件
BaO in N,N-dimethyl-formamide T=60°C; Inert atmosphere; regioselective reaction;
参考文献
Zhu, Xiangming; Dere, Ravindra T.; Jiang, Junyan; Zhang, Lei; Wang, Xiaoxia
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 10187 - 10197
反应条件
sodium methylate in methanol 0.75 h; Ambient temperature;
参考文献
Schmidt, Richard R.; Michel, Josef; Ruecker, Ernst
Liebigs Annalen der Chemie, 1989 , p. 423 - 428
反应条件
silver carbonate in benzene Heating;
参考文献
Ito, Hiroshi; Eby, Ronald; Kramer, Steven; Schuerch, Conrad
Carbohydrate Research, 1980 , vol. 86, p. 193 - 202
反应条件
potassium hydroxide in dimethyl sulfoxide 20 h; Ambient temperature;
参考文献
Tolstikov, G. A.; Valeev, F. A.; Ibragimova, I. P.; Gaisina, I. N.; Spirikhin, L. V.; Miftakhov, M. S.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 9.1 p. 1501 - 1506
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 9 p. 1875 - 1882
反应条件
1: 3.1 g / potassium tert-butoxide / toluene / 23 h / Heating 2: hydrochloride (M) / dioxane / 2 h / Heating 3: 100 percent / HCl / diethyl ether / Ambient temperature 4: silver carbonate / benzene / Heating View Scheme
参考文献
Ito, Hiroshi; Eby, Ronald; Kramer, Steven; Schuerch, Conrad
Carbohydrate Research, 1980 , vol. 86, p. 193 - 202
反应条件
1: hydrochloride (M) / dioxane / 2 h / Heating 2: 100 percent / HCl / diethyl ether / Ambient temperature 3: silver carbonate / benzene / Heating View Scheme
参考文献
Ito, Hiroshi; Eby, Ronald; Kramer, Steven; Schuerch, Conrad
Carbohydrate Research, 1980 , vol. 86, p. 193 - 202
反应条件
1: 24 g / sodium hydride / dimethylformamide / 67 h / 120 °C 2: 3.1 g / potassium tert-butoxide / toluene / 23 h / Heating 3: hydrochloride (M) / dioxane / 2 h / Heating 4: 100 percent / HCl / diethyl ether / Ambient temperature 5: silver carbonate / benzene / Heating View Scheme
参考文献
Ito, Hiroshi; Eby, Ronald; Kramer, Steven; Schuerch, Conrad
Carbohydrate Research, 1980 , vol. 86, p. 193 - 202
反应条件
1: 100 percent / HCl / diethyl ether / Ambient temperature 2: silver carbonate / benzene / Heating View Scheme
参考文献
Ito, Hiroshi; Eby, Ronald; Kramer, Steven; Schuerch, Conrad
Carbohydrate Research, 1980 , vol. 86, p. 193 - 202
反应条件
1: 40 percent / p-TosOH / benzene / 2 h / Heating 2: 65 percent / NaOMe / methanol / 0.75 h / Ambient temperature View Scheme
参考文献
Schmidt, Richard R.; Michel, Josef; Ruecker, Ernst
Liebigs Annalen der Chemie, 1989 , p. 423 - 428
反应条件
1: 75 percent / 0.4 M NaOMe / diethyl ether; methanol / 0.75 h / Ambient temperature 2: 40 percent / p-TosOH / benzene / 2 h / Heating 3: 65 percent / NaOMe / methanol / 0.75 h / Ambient temperature View Scheme
参考文献
Schmidt, Richard R.; Michel, Josef; Ruecker, Ernst
Liebigs Annalen der Chemie, 1989 , p. 423 - 428
