(9ci)-alpha,1-二甲基-1H-苯并咪唑-2-甲醇合成路线 (共 10 条)
反应条件
hydrogenchloride 0.75 h; Heating;
参考文献
Muller, Gilles; Riehl, James P.; Schenk, Kurt J.; Hopfgartner, Gerard; Piguet, Claude; Buenzli, Jean-Claude G.
European Journal of Inorganic Chemistry, 2002 , # 12 p. 3101 - 3110
反应条件
sodium tetrahydroborate in methanol; water 1 h;
参考文献
Owen, Terence C.
Journal of Heterocyclic Chemistry, 1990 , vol. 27, # 4 p. 987 - 990
反应条件
sodium hydroxide in methanol T=20°C; 0.5 h;
参考文献
Dubey; Reddy, P.V.V. Prasada; Srinivas
Synthetic Communications, 2007 , vol. 37, # 10 p. 1675 - 1681
反应条件
sodium hydroxide in acetone
参考文献
Popov
Chemistry of Heterocyclic Compounds, 1996 , vol. 32, # 6 p. 672 - 681
反应条件
potassium hydroxide in ethanol; water 1.) 0 deg C, over 5 h, 2.) 20 deg C, 1.5 h;
参考文献
Popov
Chemistry of Heterocyclic Compounds, 1996 , vol. 32, # 6 p. 672 - 681
反应条件
1: 82 percent / TEBAC; K2CO3 / acetonitrile / 20 °C 2: 80 percent / aq. NaOH / methanol / 0.5 h / 20 °C View Scheme
参考文献
Dubey; Reddy, P.V.V. Prasada; Srinivas
Synthetic Communications, 2007 , vol. 37, # 10 p. 1675 - 1681
反应条件
1: 82 percent / 2 h / 125 - 130 °C 2: 82 percent / TEBAC; K2CO3 / acetonitrile / 20 °C 3: 80 percent / aq. NaOH / methanol / 0.5 h / 20 °C View Scheme
参考文献
Dubey; Reddy, P.V.V. Prasada; Srinivas
Synthetic Communications, 2007 , vol. 37, # 10 p. 1675 - 1681
参考文献
Phillips
Journal of the Chemical Society, 1929 , p. 2828
反应条件
1: 89 percent / KMnO4 on neutral alumina / 0.08 h / 20 °C 2: 95 percent / NaOH / 0.17 h / 20 °C View Scheme
参考文献
Dubey; Kumar, C. Ravi; Babu, Balaji
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 12 p. 3128 - 3130
反应条件
KMnO4/alumina
T=20°C; 0.0833333 h;
参考文献
Dubey; Kumar, C. Ravi; Babu, Balaji
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 12 p. 3128 - 3130