5,6-二氢-4-羟基-6-甲基-2H-吡喃-2-酮合成路线 (共 18 条)
反应条件
hydrogen; 5 Pd/Nb2O5 in butan-1-ol T=69.84°C; P=5171.62 Torr; 5 h;
参考文献
US2012/116119 A1, ;
Page/Page column 5 ;
反应条件
hydrogen; 5 Pd/Nb2O5 in isopropyl alcohol T=49.84°C; P=5171.62 Torr; 5 h; Product distribution / selectivity;
参考文献
US2012/116119 A1, ;
Page/Page column 5 ;
反应条件
palladium 10 on activated carbon in tetrahydrofuran T=49.84°C; P=25858.1 Torr; 8 h;
参考文献
US2012/116119 A1, ;
Page/Page column 6 ;
反应条件
water in 1,4-dioxane 2 h; Heating; Yield given;
参考文献
Monatshefte fuer Chemie, , vol. 113, p. 1213 - 1216
反应条件
1: NaHCO3, NaBH4 / CH2Cl2 / 3 h 2: H2O / dioxane / 2 h / Heating View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 113, p. 1213 - 1216
反应条件
tetra(n-butyl)ammonium hydroxide in methanol Isomerization; 0.333333 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 34, # 9 p. 1350 - 1354
反应条件
water T=25°C; Rate constantMechanism;
参考文献
Journal of Pharmaceutical Sciences, , vol. 79, # 2 p. 138 - 146
反应条件
hydrogen; platinum in ethyl acetate P=760 Torr; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 21, p. 551 - 554
反应条件
in water T=179.84°C; P=25858.1 Torr; Inert atmosphere; Product distribution / selectivity;
参考文献
Dumesic, James A.; Chia, Mei
Patent: US2012/116119 A1, 2012 ;
Location in patent: Page/Page column 6 ;
反应条件
Amberlyst 70 in water T=69.84°C; 1 h;
参考文献
Journal of the American Chemical Society, , vol. 135, # 15 p. 5699 - 5708