5,5-二甲基-1-吡咯啉-N-氧化物合成路线 （共 38 条）
反应条件
sodium hydride in ethylene glycol dimethyl ether
T=25°C; 3.5 h;
参考文献
Zbaida, Shmuel; Breuer, Eli
Journal of Organic Chemistry, 1982 , vol. 47, # 6 p. 1073 - 1077
反应条件
n-butyllithium in tetrahydrofuran
T=64°C; 24 h;
参考文献
Zbaida, Shmuel; Breuer, Eli
Journal of Organic Chemistry, 1982 , vol. 47, # 6 p. 1073 - 1077
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=25°C; other nitrone; Mechanism;
参考文献
Bapat, Jayant Bhalchandra; Durie, Alexander
Australian Journal of Chemistry, 1984 , vol. 37, # 1 p. 211 - 219
反应条件
1: 67 percent / diethyl ether / 0.5 h / Heating
2: 65 percent / O2, Cu-acetate, NH3 / aq. ethanol
View Scheme
参考文献
Janzen, Edward G.; Zhang, Yong-Kang; Haire, D. Lawrence
Magnetic Resonance in Chemistry, 1994 , vol. 32, # 12 p. 711 - 720
反应条件
ammonium hydroxide; oxygen; copper diacetate
1.) Et2O, r.t., overnight, 2.) MeOH; Yield given. Multistep reaction;
参考文献
Janzen, Edward G.; Zhang, Yong-Kang; Haire, D. Lawrence
Magnetic Resonance in Chemistry, 1994 , vol. 32, # 12 p. 711 - 720
反应条件
ammonium hydroxide; air; copper diacetate
2.) MeOH; Multistep reaction;
参考文献
Janzen, Edward G.; Zhang, Yong-Kang
Journal of Magnetic Resonance, Series B, 1993 , vol. 101, # 1 p. 91 - 93
反应条件
in diethyl ether
0.5 h; Heating;
参考文献
Aurich, Hans Guenter; Franzke, Michael; Kesselheim, Hans Peter; Rohr, Markus
Tetrahedron, 1992 , vol. 48, # 4 p. 669 - 682
反应条件
1: 2.) copper(II) acetate monohydrate, 28percent aq. NH3, O2 / 1.) Et2O, r.t., overnight, 2.) MeOH
2: LiAlH4 / diethyl ether / 1.5 h / 0 - 5 °C
View Scheme
参考文献
Janzen, Edward G.; Zhang, Yong-Kang; Haire, D. Lawrence
Magnetic Resonance in Chemistry, 1994 , vol. 32, # 12 p. 711 - 720
反应条件
1: 2.) copper(II) acetate monohydrate, 28percent aq. NH3, O2 / 1.) Et2O, r.t., overnight, 2.) MeOH
2: LiAlH4 / diethyl ether / 1.5 h / 0 - 5 °C
View Scheme
参考文献
Janzen, Edward G.; Zhang, Yong-Kang; Haire, D. Lawrence
Magnetic Resonance in Chemistry, 1994 , vol. 32, # 12 p. 711 - 720
反应条件
methanol; selenium(IV) oxide
参考文献
Clark et al.
Journal of the Chemical Society, 1959 , p. 2123,2126
