1-(2-甲氧苯基)-2-硝基乙烯合成路线 (共 8 条)
反应条件
O-(tert-butyldiphenylsilyl)-L-tyrosine lithium salt; magnesium sulfate in dichloromethane T=25°C; 24 h; stereoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 76, # 7 p. 2305 - 2309
反应条件
bis(α-ethylphenylamine) copper acetate in methanol T=20°C; Henry reaction; 72 h; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Letters, , vol. 51, # 42 p. 5577 - 5580
反应条件
AgNO2; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in 1,2-dichloro-ethane T=70°C; 12 h; Molecular sieve; stereoselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 135, # 9 p. 3355 - 3358
反应条件
tert.-butylnitrite; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in acetonitrile T=50°C; 3 h; stereoselective reaction;
参考文献
Chemical Communications, , vol. 49, # 46 p. 5286 - 5288
反应条件
1: pyridine / 2 h / Ambient temperature 2: sodium carbonate / benzene / 5 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 11 p. 4029 - 4036
反应条件
1: triethylamine / 17 h 2: pyridine / 2 h / Ambient temperature 3: sodium carbonate / benzene / 5 h / Heating View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 11 p. 4029 - 4036
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 986 - 990
反应条件
tert.-butylhydroperoxide; n-butyllithium in tetrahydrofuran; hexane; toluene
T=-20°C; 1.5 h;
参考文献
Ashwell, Mark A.; Jackson, Richard F. W.
Synthesis, 1988 , # 3 p. 229 - 231