2-甲基-3H-苯并[4,5]呋喃并[3,2-d]嘧啶-4-酮合成路线 (共 16 条)
反应条件
potassium hydroxide in ethanol; water 5 h; Heating;
参考文献
Takagi, Kaname; Hubert-Habart, Michel
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 9-10 p. 444 - 448
反应条件
potassium hydroxide in ethanol; water 5 h; Heating;
参考文献
Takagi, Kaname; Hubert-Habart, Michel
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 9-10 p. 444 - 448
反应条件
1: 79 percent / sulfuryl chloride / CHCl3 / 2 h, room temperature then 1 h, reflux 2: 11 percent / sodium ethoxide / ethanol / 7 h / Heating 3: 47 percent / KOH / ethanol; H2O / 5 h / Heating View Scheme
参考文献
Takagi, Kaname; Hubert-Habart, Michel
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 9-10 p. 444 - 448
反应条件
potassium hydroxide in ethanol 0.666667 h; Heating;
参考文献
Vaidya, V. P.; Agasimundin, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 9 p. 780 - 783
反应条件
1: 11 percent / sodium ethoxide / ethanol / 7 h / Heating 2: 47 percent / KOH / ethanol; H2O / 5 h / Heating View Scheme
参考文献
Takagi, Kaname; Hubert-Habart, Michel
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 9-10 p. 444 - 448
反应条件
1: 11 percent / sodium ethoxide / ethanol / 7 h / Heating 2: 57 percent / KOH / ethanol; H2O / 5 h / Heating View Scheme
参考文献
Takagi, Kaname; Hubert-Habart, Michel
Bulletin de la Societe Chimique de France, 1980 , vol. 2, # 9-10 p. 444 - 448
反应条件
1: 25 percent / hydrazine hydrate (80percent) / ethanol / 1.5 h / Heating 2: 1.) aq. HOAc (50percent) 2.) NaNO2 / 1.) 45-50 deg C 2.) heating at the same temp. until evolution of brown fumes ceased View Scheme
参考文献
Mahajan, S. B.; Agasimundin, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 5 p. 402 - 404
反应条件
1: 81 percent / 0.08 h / Heating 2: 91.5 percent / 2 N aqueous sodium hydroxide / 4 h / Heating 3: 63 percent / H2O / 2 h / water-bath 4: potassium hydroxide / ethanol / 0.67 h / Heating View Scheme
参考文献
Vaidya, V. P.; Agasimundin, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 9 p. 780 - 783
反应条件
1: 63 percent / H2O / 2 h / water-bath 2: potassium hydroxide / ethanol / 0.67 h / Heating View Scheme
参考文献
Vaidya, V. P.; Agasimundin, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 9 p. 780 - 783
反应条件
1: 91.5 percent / 2 N aqueous sodium hydroxide / 4 h / Heating 2: 63 percent / H2O / 2 h / water-bath 3: potassium hydroxide / ethanol / 0.67 h / Heating View Scheme
参考文献
Vaidya, V. P.; Agasimundin, Y. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 9 p. 780 - 783