反应条件
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / Reflux; Inert atmosphere 2: titanium tetrachloride; triethylamine / toluene / 12 h / 0 - 20 °C / Inert atmosphere 3: (R)-N-(phenylcarbamoyl)-tert-butanesulfinamide; trichlorosilane; water / acetonitrile / 24 h / -40 °C 4: ammonium cerium (IV) nitrate; water / acetonitrile / 0.5 h / 0 °C 5: acetonitrile / 12 h / 20 °C 6: acetic acid; sodium nitrite / dimethyl sulfoxide / 24 h / 40 °C / Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 18, # 30 p. 9204 - 9207