(S)-2-(苄氧基)-1-丙醇合成路线 （共 33 条）
反应条件
1: 95 percent / 50percent acetic acid / 1 h / Heating 2: 91 percent / NaBH4 / H2O / 3 h / Ambient temperature 3: 75 percent / NaIO4 / ethanol; H2O / 0.25 h / Ambient temperature 4: 94 percent / NaBH4 / ethanol / 0.75 h / Ambient temperature View Scheme
参考文献
Liebigs Annalen der Chemie, , # 3 p. 372 - 377
反应条件
1: 1.) O3, 2.) (C6H5)3P / 1.) CH2Cl2, -40 deg C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 49, # 3 p. 543 - 546
反应条件
sodium tetrahydroborate; dimethylsulfide; ozone Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 31, # 43 p. 6239 - 6242
反应条件
sodium tetrahydroborate; ozone 1.) CH3OH, CH2Cl2, -78 deg C, 30 min, 2,) CH3OH, CH2Cl2, from -78 deg C to RT; Yield given. Multistep reaction;
参考文献
Tetrahedron Asymmetry, , vol. 8, # 22 p. 3801 - 3805
反应条件
lithium aluminium tetrahydride
参考文献
Helvetica Chimica Acta, , vol. 54, # 3 p. 845 - 851
反应条件
1: 60 percent KOH / 2 h / Heating 2: 2.) lithium aluminum hydride / 1.) Glomerella cingulata ( Malus spp. ) culture containing peptone, KH2PO4, sucrose and MgSO4*7H2O; pH = 5.5, water, 27 deg C, 20 d; 2.) ether, 2 h, ref. View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 33, # 11 p. 4657 - 4661
反应条件
lithium aluminium tetrahydride 1.) Glomerella cingulata ( Malus spp. ) culture containing peptone, KH2PO4, sucrose and MgSO4*7H2O; pH = 5.5, water, 27 deg C, 20 d; 2.) ether, 2 h, ref.; Multistep reaction. Title compound not separated from byproducts;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 33, # 11 p. 4657 - 4661
反应条件
lipase-PS in hexane T=25°C; 1 h; Product distribution; Further Variations:CatalystsSolvents;
参考文献
Chemistry Letters, , vol. 34, # 5 p. 682 - 683
反应条件
Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 123, p. C25 - C28
反应条件
racemate resolution; kinetc resolution via acetylation with vinyl acetate catalysed by lipase PS; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 10, # 20 p. 3939 - 3949
