(S)-2-(苄氧基)-1-丙醇合成路线 (共 33 条)
反应条件
lithium aluminium tetrahydride in diethyl ether T=0 - 20°C; 2 h;
参考文献
Suzuki, Yumiko; Wakatsuki, Junichiro; Tsubaki, Mariko; Sato, Masayuki
Tetrahedron, 2013 , vol. 69, # 46 p. 9690 - 9700
反应条件
lithium aluminium tetrahydride
参考文献
Desert, Stephane; Metzner, Patrick
Tetrahedron, 1992 , vol. 48, # 47 p. 10327 - 10338
反应条件
1: With ozone in methanol T=-78°C; 0.0127778 h; 2: With sodium tetrahydroborate in methanol T=0 - 20°C;
参考文献
Wee, Andrew G. H.; Shi, Qing; Wang, Zhongyi; Hatton, Kimberly
Tetrahedron Asymmetry, 2003 , vol. 14, # 7 p. 897 - 909
反应条件
palladium dichloride in methanol T=20°C; 4 h;
参考文献
Sugawara, Fumio; Nakayama, Haruhiko; Stroebel, Gary A.; Ogawa, Tomoya
Agricultural and Biological Chemistry, 1986 , vol. 50, # 9 p. 2261 - 2272
反应条件
sodium tetrahydroborate in ethanol T=0°C; 2 h;
参考文献
Kobayashi; Takase; Ito; Terashima
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 9 p. 3038 - 3040
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
参考文献
Helmchen, Guenter; Wierzchowski, Reiner
Angewandte Chemie, 1984 , vol. 96, # 1 p. 59 - 60
反应条件
1: 69 percent / silver oxide / diethyl ether / Heating 2: 96 percent / LiBH4 / tetrahydrofuran / -17 - 20 °C View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 12 p. 1878 - 1881
反应条件
1: 11.8 mmol / CF3SO3H / tetrahydrofuran / 18 h / 20 °C 2: 98 percent / LiAlH4 / tetrahydrofuran / 1.5 h / 23 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 342, # 7 p. 654 - 658
反应条件
1.1: NaH / diethyl ether / 20 °C 1.2: diethyl ether / 1.5 h / 20 °C 2.1: 11.8 mmol / CF3SO3H / tetrahydrofuran / 18 h / 20 °C 3.1: 98 percent / LiAlH4 / tetrahydrofuran / 1.5 h / 23 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 342, # 7 p. 654 - 658
反应条件
borane-THF in tetrahydrofuran T=0°C; 1 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Liebigs Annales, , # 1 p. 11 - 26