7,8-二氮杂双环[2.2.2]辛-7-烯合成路线 （共 17 条）
反应条件
in methanol-d4 0.25 h; Ambient temperatureIrradiation;
参考文献
Gramlich, Gabriela; Nau, Werner M.
Organic Letters, 1999 , vol. 1, # 4 p. 603 - 605
反应条件
1: 98 percent / H2 / Pd/C / ethanol / 2 h / atmospheric pressure 2: 100 percent / hexane / UV-irradiation View Scheme
参考文献
Squillacote, Michael; Felippis, James De
Journal of Organic Chemistry, 1994 , vol. 59, # 13 p. 3564 - 3571
反应条件
sodium hydroxide; [NO][PF6]; acetonitrile 1.) r.t., 30 min, 2.) 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nelsen, Stephen F.; Wang, Yichun
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3082 - 3090
反应条件
pyridine; sodium hydroxide 1.) ether, 2.) toluene, 0 deg C to r.t., overnight; Yield given;
参考文献
Nelsen, Stephen F.; Kim, Yaesil; Neugebauer, Franz A.; Krieger, Claus; Siegel, Rolf; Kaftory, Menahem
Journal of Organic Chemistry, 1991 , vol. 56, # 3 p. 1045 - 1051
反应条件
sodium hydroxide; [NO][PF6] 1.) r.t., 30 min, 2.) 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Nelsen, Stephen F.; Wang, Yichun
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3082 - 3090
反应条件
methanol; potassium hydroxide; palladium on activated charcoal Hydrogenation.anschl. mit CuCl2 in H2O und Behandeln der erhaltenen Verbindung mit CuCl und wss. KOH;
参考文献
Pirsch; Joergl
Chemische Berichte, 1935 , vol. 68, p. 1324,1329
反应条件
Aufbewahren an der Luft;
参考文献
Pirsch; Joergl
Chemische Berichte, 1935 , vol. 68, p. 1324,1329
反应条件
2,6-di-tert-butyl-pyridine in acetonitrile T=25°C; further cation radical reagent; novel oxaditive azoalkane reaction; Product distributionMechanism;
参考文献
Engel, Paul S.; Hoque, A. K. M. M.; Scholz, John N.; Shine, Henry J.; Whitmire, Kenton H.
Journal of the American Chemical Society, 1988 , vol. 110, # 23 p. 7880 - 7882
反应条件
2,6-di-tert-butyl-4-methylpyridine in acetonitrile T=25°C;
参考文献
Journal of the American Chemical Society, , vol. 110, # 23 p. 7880 - 7882
反应条件
in pentane 0.0833333 h; Irradiationλ = 185 nm; other times, λ; Product distributionQuantum yield;
参考文献
Engel, Paul S.; Horsey, Douglas W.; Keys, Dalen E.; Nalepa, Christopher J.; Soltero, Luis R.
Journal of the American Chemical Society, 1983 , vol. 105, # 24 p. 7108 - 7114
