N'-Cbz-L-鸟氨酸合成路线 （共 19 条）
反应条件
1: L-(+)-ornithine hydrochloride With sodium hydroxide in water 2: With CuSO4‵5H2O in water 0.25 h; 3: benzyl chloroformate Further stages;
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 52, # 2 p. 29 - 32
反应条件
1: L, 5 diaminopentanoic acid With cupric(II) carbonate in water 0.5 h; 2: benzyl chloroformate With sodium hydroxide in water 1 h; 3: With hydrogenchloride; ethylenediaminetetraacetic acid 2 h; Further stages.;
参考文献
Chemical Communications, , # 8 p. 717 - 718
反应条件
mold acylase in water; triethylamine T=38°C; 168 h; pH 7.4;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 2 p. 575 - 576
反应条件
sodium hydroxide in water T=20°C; 0.5 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 10 p. 3103 - 3108
反应条件
1: 90 percent / Et3N / acetonitrile / 2 h / 5 °C 2: 80 percent / 2M NaOH / H2O / 0.5 h / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 62, # 10 p. 3103 - 3108
反应条件
1: 1.) 2N LiOH / 1.) -5 deg C, 2.) 0 deg C 2: 1.) 1N NaOH, 2.) 1N NaOH / 1.) -3 deg C, 2.) -3 deg C View Scheme
参考文献
Synthetic Communications, , vol. 21, # 1 p. 99 - 105
反应条件
sodium hydroxide 1.) -3 deg C, 2.) -3 deg C; Multistep reaction;
参考文献
Synthetic Communications, , vol. 21, # 1 p. 99 - 105
反应条件
2: HBr; acetic acid 3: aqueous NaOH 4: HBr; acetic acid; phenol View Scheme
参考文献
Zaoral; Rudinger
Collection of Czechoslovak Chemical Communications, 1959 , vol. 24, p. 1993,2002
反应条件
sodium hydrogencarbonate in 1,4-dioxane; water T=23°C; 24 h;
参考文献
Feldman
Tetrahedron Letters, 1991 , vol. 32, # 7 p. 875 - 878
反应条件
triethylamine in tert-butyl alcohol
参考文献
Broadbent,W. et al.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 2632 - 2636
