2-(2-羟基丙-2-基)-5-甲基环己烷-1-酮合成路线 （共 6 条）
反应条件
1: 3(R)-methylcyclohexanone With n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: acetone in tetrahydrofuran; hexane T=-78°C; 1 h; Further stages.;
参考文献
Bartoli, Giuseppe; Bosco, Marcella; Dalpozzo, Renato; Giuliani, Arianna; Marcantoni, Enrico; Mecozzi, Tiziana; Sambri, Letizia; Torregiani, Elisabetta
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 9111 - 9114
反应条件
chromium(VI) oxide; sulfuric acid in water
参考文献
Von Poser, Gilsane L.; Menut, Chantal; Toffoli, Maria E.; Verin, Pierre; Sobral, Marcos; Bessiere, Jean-Marie; Lamaty, Gerard; Henriques, Amelia T.
Journal of Agricultural and Food Chemistry, 1996 , vol. 44, # 7 p. 1829 - 1832
反应条件
1: m-chloroperbenzoic acid / CHCl3 / 24 h / Ambient temperature 2: 70 percent / AlLiH4 / diethyl ether / 1 h / 40 °C 3: CrO3, concd. H2SO4 / H2O View Scheme
参考文献
Von Poser, Gilsane L.; Menut, Chantal; Toffoli, Maria E.; Verin, Pierre; Sobral, Marcos; Bessiere, Jean-Marie; Lamaty, Gerard; Henriques, Amelia T.
Journal of Agricultural and Food Chemistry, 1996 , vol. 44, # 7 p. 1829 - 1832
反应条件
1: 70 percent / AlLiH4 / diethyl ether / 1 h / 40 °C 2: CrO3, concd. H2SO4 / H2O View Scheme
参考文献
Von Poser, Gilsane L.; Menut, Chantal; Toffoli, Maria E.; Verin, Pierre; Sobral, Marcos; Bessiere, Jean-Marie; Lamaty, Gerard; Henriques, Amelia T.
Journal of Agricultural and Food Chemistry, 1996 , vol. 44, # 7 p. 1829 - 1832
反应条件
cerium(III) chloride; sodium iodide in acetonitrile 2 h; Heating;
参考文献
Bartoli, Giuseppe; Bosco, Marcella; Dalpozzo, Renato; Giuliani, Arianna; Marcantoni, Enrico; Mecozzi, Tiziana; Sambri, Letizia; Torregiani, Elisabetta
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 9111 - 9114
反应条件
cerium(III) chloride; sodium iodide in acetonitrile
2 h; Heating;
参考文献
Bartoli, Giuseppe; Bosco, Marcella; Dalpozzo, Renato; Giuliani, Arianna; Marcantoni, Enrico; Mecozzi, Tiziana; Sambri, Letizia; Torregiani, Elisabetta
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 9111 - 9114
