1: With 1,3-bis-(diphenylphosphino)propane; triethylamine; palladium diacetate in various solvent(s) T=125°C; Regioselective Heck arylation; 30 h; 2: With hydrogenchloride in various solvent(s) 1 h;
参考文献
Pei, Wen; Mo, Jun; Xiao, Jianliang
Journal of Organometallic Chemistry, 2005 , vol. 690, # 15 p. 3546 - 3551
1: With triphenylphosphine in acetonitrile T=20°C; 4 h; Inert atmosphere; 2: With hydrogenchloride in water; acetonitrile 0.0833333 h; Inert atmosphere;
参考文献
Khong, San; Kwon, Ohyun
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8257 - 8267,11
1: With triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in toluene T=110°C; Stille coupling reaction; 1 h; 2: With hydrogenchloride in toluene T=20°C; 24 h;
1: methyllithium With indium(III) chloride in tetrahydrofuran; hexane T=-78 - 20°C; 2: 3-(bromo)-quinoline; carbon monoxide With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane T=60°C; 2 h;
参考文献
Lee, Sung Wook; Lee, Kooyeon; Seomoon, Dong; Kim, Sundae; Kim, Hyunseok; Kim, Hyun; Shim, Eunkyong; Lee, Miae; Lee, Seokju; Kim, Misook; Lee, Phil Ho
Journal of Organic Chemistry, 2004 , vol. 69, # 14 p. 4852 - 4855
1: With bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=70°C; Negishi coupling reaction; 48 h; 2: With hydrogenchloride in tetrahydrofuran T=20°C; 24 h;
1: With triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=70°C; Negishi coupling reaction; 48 h; 2: With hydrogenchloride in tetrahydrofuran T=20°C; 24 h;