5-苯基噁唑-4-羧酸乙酯合成路线 （共 15 条）
反应条件
P(t-Bu)2Me*HBF4; palladium diacetate; caesium carbonate in 1,4-dioxane T=110°C; 18 h; Inert atmosphere; Reagent/catalyst;
参考文献
Theveau, Laure; Querolle, Olivier; Dupas, Georges; Hoarau, Christophe
Tetrahedron, 2013 , vol. 69, # 22 p. 4375 - 4380
反应条件
palladium diacetate; caesium carbonate; 2-dicyclohexylphosphino-1,1'-biphenyl in 1,4-dioxane T=110°C; 18 h; Inert atmosphere; Reagent/catalyst;
参考文献
Theveau, Laure; Querolle, Olivier; Dupas, Georges; Hoarau, Christophe
Tetrahedron, 2013 , vol. 69, # 22 p. 4375 - 4380
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran T=10 - 20°C; 18 h;
参考文献
Ladouceur, Gaetan H.; Schoen, William R.; Burke, Michael J.
Patent: US2003/195352 A1, 2003 ;
Location in patent: Page/Page column 35 ;
反应条件
1: isocyano-acetic acid ethyl ester With sodium hydride in benzene T=20°C; 2 h; 2: benzoyl chloride in benzene T=20°C; 24 h;
参考文献
Tormyshev; Mikhalina; Rogozhnikova; Troitskaya; Trukhin
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 7 p. 1031 - 1035
反应条件
copper(I) oxide; triethylamine in tetrahydrofuran 14 h; Ambient temperature;
参考文献
Kozikowski, Alan P.; Ames, Anthony
Journal of the American Chemical Society, 1980 , vol. 102, # 2 p. 860 - 862
反应条件
palladium diacetate; potassium carbonate; PCy3∙HBF4; 2,2,2-trimethylacetic acid in 1,4-dioxane T=110°C; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Theveau, Laure; Verrier, Cecile; Lassalas, Pierrik; Martin, Thibaut; Dupas, Georges; Querolle, Olivier; Van Hijfte, Luc; Marsais, Francis; Hoarau, Christophe
Chemistry - A European Journal, 2011 , vol. 17, # 51 p. 14450 - 14463
反应条件
palladium diacetate; caesium carbonate; tris-(o-tolyl)phosphine in carbonic acid diethyl ester T=110°C; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Dong, Jia Jia; Roger, Julien; Verrier, Cecile; Martin, Thibaut; Le Goff, Ronan; Hoarau, Christophe; Doucet, Henri
Green Chemistry, 2010 , vol. 12, # 11 p. 2053 - 2063
反应条件
palladium diacetate; potassium carbonate; [(t-Bu)3PH]BF4; 2,2,2-trimethylacetic acid in toluene T=110°C; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Chemistry - A European Journal, , vol. 17, # 51 p. 14450 - 14463
反应条件
palladium diacetate; potassium carbonate; [(t-Bu)3PH]BF4 in 1,4-dioxane T=110°C; 18 h; Inert atmosphere; regioselective reaction;
参考文献
Chemistry - A European Journal, , vol. 17, # 51 p. 14450 - 14463
