环戊二烯基双(三苯基膦)氯化钌(II)合成路线 (共 32 条)
反应条件
air in methanol
byproducts: TlCl; equimolar mixt. of Tl salt and Ru-complex in MeOH was stirred for 2 h at 60°C in air; filtered, washed with MeOH, combined filtrates cooled overnight at -30°C; elem. anal.;
参考文献
Bruce, Michael I.; Wallis, Robert C.; Williams, Michael L.; Skelton, Brian W.; White, Allan H.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1983 , p. 2183 - 2190
反应条件
air in methanol
refluxing CpRuCl(PPh3)2 in methanol for 0.5 h, cooling; filtration, evapn. of the filtrate to dryness, not isolated;
参考文献
Wilczewski, Tadeusz
Journal of Organometallic Chemistry, 1990 , vol. 382, # 3 p. 431 - 443