6-氯-3-乙基-2-丙基喹啉合成路线 (共 6 条)
反应条件
AlCl3, aluminium chloride; dihydrogen peroxide in dichloromethane; water T=25°C; Inert atmosphere;
参考文献
Guo, Qiaoxia; Wang, Wennian; Teng, Weiling; Chen, Liwei; Wang, Yanqing; Shen, Baojian
Synthetic Communications, 2012 , vol. 42, # 17 p. 2574 - 2584
反应条件
1-hexene; bis(1,1-diphenylphosphino)methane; tin(ll) chloride; ruthenium trichloride in 1,4-dioxane T=180°C; Cyclization; Alkylation; 20 h;
参考文献
Cho, Chan Sik; Oh, Byoung Ho; Kim, Joon Seok; Kim, Tae-Jeong; Shim, Sang Chul
Chemical Communications (Cambridge, United Kingdom), 2000 , # 19 p. 1885 - 1886
反应条件
tin(ll) chloride; tris(triphenylphosphine)ruthenium(II) chloride in water; toluene T=180°C; 20 h;
参考文献
Cho, Chan Sik; Kim, Tae Kyung; Kim, Bok Tae; Kim, Tae-Jeong; Shim, Sang Chul
Journal of Organometallic Chemistry, 2002 , vol. 650, # 1-2 p. 65 - 68
反应条件
carbon monoxide; RhCl(PPh3)3; water; palladium dichloride in ethanol T=180°C; P=53200 Torr; 4 h;
参考文献
Watanabe, Yoshihisa; Suzuki, Naoki; Tsuji, Yasushi; Shim, Sang Chul; Mitsudo, Take-aki
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 4 p. 1116 - 1120
反应条件
FeCl3*6H2O in tetrachloromethane T=140°C; 4 h; AutoclaveInert atmosphereSealed tube;
参考文献
Khusnutdinov; Bayguzina; Aminov
Russian Chemical Bulletin, 2013 , vol. 62, # 1 p. 133 - 137
Izv. Akad. Nauk, Ser. Khim., 2013 , # 1 p. 134 - 138
反应条件
ruthenium trichloride T=180°C; 4 h; high pressure, under argon;
参考文献
Watanabe; Tsuji; Shida
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 2 p. 435 - 438