1,2,3,4-四氢吖啶合成路线 (共 54 条)
反应条件
benzophenone; potassium tert-butylate in 1,4-dioxane T=90°C; Friedlaender synthesis; 0.5 h; Inert atmosphere;
参考文献
Martinez, Ricardo; Ramon, Diego J.; Yus, Miguel
Journal of Organic Chemistry, 2008 , vol. 73, # 24 p. 9778 - 9780
反应条件
1: With triethylamine; L-proline in dichloromethane T=20°C; Inert atmosphere; 2: With triphenylphosphine in dichloromethane T=20°C; Inert atmosphere;
参考文献
Yu, Zhi-Hua; Zheng, Hu-Fei; Yuan, Wei; Tang, Zi-Long; Zhang, Ai-Dong; Shi, De-Qing
Tetrahedron, 2013 , vol. 69, # 38 p. 8137 - 8141
反应条件
hydrogen; palladium/alumina in ethanol T=100°C; P=53200 Torr; 15 h; other catalysts; Further byproducts given;
参考文献
Chemistry Letters, , # 2 p. 319 - 322
反应条件
{(S)-1-[(R)-(diphenylphosphino)ferrocenyl]}ethyl-di-tert-butylphosphine; palladium diacetate; sodium t-butanolate in ethylene glycol dimethyl ether T=100°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 52, # 8 p. 916 - 919
反应条件
{(S)-1-[(R)-(diphenylphosphino)ferrocenyl]}ethyl-di-tert-butylphosphine; palladium diacetate; sodium t-butanolate in ethylene glycol dimethyl ether T=100°C; 18 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 52, # 8 p. 916 - 919
反应条件
hydrogen; palladium on activated charcoal in methanol T=18°C; P=760 Torr; 2 h;
参考文献
Banwell, Martin G.; Lupton, David W.; Ma, Xinghua; Renner, Jens; Sydnes, Magne O.
Organic Letters, 2004 , vol. 6, # 16 p. 2741 - 2744
反应条件
{(S)-1-[(R)-(diphenylphosphino)ferrocenyl]}ethyl-di-tert-butylphosphine; palladium diacetate; sodium t-butanolate in ethylene glycol dimethyl ether T=100°C; 24 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 52, # 8 p. 916 - 919
反应条件
hydrogen; palladium/alumina in ethanol T=100°C; P=53200 Torr; 15 h; other catalysts; Further byproducts given;
参考文献
Chemistry Letters, , # 2 p. 319 - 322
反应条件
hydrogen; palladium/alumina in decalin T=150°C; P=53200 Torr; 0.166667 h; Further byproducts given;
参考文献
Sakanishi, Kinya; Ohira, Masato; Mochida, Isao; Okazaki, Hiroshi; Soeda, Mahito
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1769 - 1774
反应条件
hydrogen; Wilkinson's catalyst in benzene T=85°C; P=16031.6 Torr; rates (percent/min) and relative rates of hydrogenation;
参考文献
Journal of Organic Chemistry, , vol. 49, # 23 p. 4500 - 4505