反应条件
in hexane Kinetics; byproducts: CoCl2, HgCl2, tetrachloroethylene; under N2 stirred at 30°C for 5 h; filtered for CoCl2, HgCl2, HgPhCl, HgPh2, filtrate concd., chromy. (pentane), distd. for Cl2CCCl2, product yield dependence to various reagents, react. at 60°C for 2 h gave <Co(CO)12>;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 403 - 406