3-(三氟甲基)异氰酸苯酯合成路线 (共 25 条)
反应条件
triethylamine in benzene Condensation; 3 h; Heating;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 39, # 1 p. 76 - 79
反应条件
in toluene T=15 - 20°C; 1 h;
参考文献
Russian Journal of General Chemistry, , vol. 76, # 1 p. 110 - 115
反应条件
in 1,4-dioxane Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 29, # 7 p. 1302 - 1305
反应条件
in toluene 2 h; Ambient temperature;
参考文献
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), , vol. 341, # 4 p. 332 - 341
反应条件
triethylamine T=10°C; 2 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 16, # 17 p. 8187 - 8195
反应条件
1: 97 percent / H2SO4 / 1 h / 170 - 175 °C 2: 89 percent / toluene / 1 h / 15 - 20 °C View Scheme
参考文献
Russian Journal of General Chemistry, , vol. 76, # 1 p. 110 - 115
反应条件
in toluene T=0°C; Reflux;
参考文献
Asian Journal of Chemistry, , vol. 25, # 4 p. 2149 - 2152
反应条件
T=170 - 220°C; ΔH; heat of dissociation; Thermodynamic data;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 54, # 7 p. 1477 - 1481,1317 - 1320
反应条件
triethylamine in dimethyl sulfoxide 24 h; Ambient temperature;
参考文献
Lombardino,J.G.; Wisemann,E.H.
Journal of Medicinal Chemistry, 1971 , vol. 14, p. 973 - 977