2,3,4,6-四氟苯甲酸合成路线 （共 13 条）
反应条件
sulfuric acid
68 h; Heating;
参考文献
Domagala; Bridges; Culbertson; Gambino; Hagen; Karrick; Porter; Sanchez; Sesnie; Spense; Szotek; Wemple
Journal of Medicinal Chemistry, 1991 , vol. 34, # 3 p. 1142 - 1154
反应条件
ammonia; sodium
T=-45°C; Reduction; Hydrodefluorination; 0.25 h; Title compound not separated from byproducts;
参考文献
Konovalov, Valery V.; Laev, Sergey S.; Beregovaya, Irina V.; Shchegoleva, Lyudmila N.; Shteingarts, Vitalij D.; Tsvetkov, Yuri D.; Bilkis, Itzhak
Journal of Physical Chemistry A, 2000 , vol. 104, # 2 p. 352 - 361
反应条件
1: 9 percent Spectr. / Zn; NH3 / -45 °C
2: 9 percent Spectr. / Na; NH3 / 0.25 h / -45 °C
View Scheme
参考文献
Konovalov, Valery V.; Laev, Sergey S.; Beregovaya, Irina V.; Shchegoleva, Lyudmila N.; Shteingarts, Vitalij D.; Tsvetkov, Yuri D.; Bilkis, Itzhak
Journal of Physical Chemistry A, 2000 , vol. 104, # 2 p. 352 - 361
