叔丁氧羰基-(O-苄基)谷氨酰-琥珀酰亚胺合成路线 （共 6 条）
反应条件
dicyclohexyl-carbodiimide in ethylene glycol dimethyl ether T=5°C; 18 h;
参考文献
Hoekstra, William J.; Sunder, Shyam S.; Cregge, Robert J.; Ashton, Louis A.; Stewart, Kenneth T.; King, Chi-Hsin R.
Tetrahedron, 1992 , vol. 48, # 2 p. 307 - 318
反应条件
dicyclohexyl-carbodiimide in 1,4-dioxane; ethyl acetate T=0°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 103, # 21 p. 6373 - 6377
反应条件
pyridine in acetonitrile T=20°C; 1.5 h; further solvent, base;
参考文献
Il'ina, A. V.; Davidovich, Yu. A.; Rogozhin, S. V.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1067 - 1070
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 5 p. 1163 - 1165
反应条件
N,N-dicyclohexylamine in acetonitrile T=20°C; 1.5 h; further solvent, base;
参考文献
Il'ina, A. V.; Davidovich, Yu. A.; Rogozhin, S. V.; Moiseenkov, A. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1067 - 1070
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 5 p. 1163 - 1165
反应条件
1: 97 percent / triethylamine / dioxane; H2O / 0 - 20 °C 2: 0.38 g / 1,3-dicyclohexylcarbodiimide / ethyl acetate / 17 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 2 p. 501 - 517
反应条件
1: 97 percent / triethylamine / dioxane; H2O / 0 - 20 °C 2: 0.38 g / 1,3-dicyclohexylcarbodiimide / ethyl acetate / 17 h / 20 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 13, # 2 p. 501 - 517
