O,O-二乙基 S-甲基二硫代磷酸酯合成路线 （共 16 条）
反应条件
1: O,O-diethyl chlorothiophosphate With ammonia; potassium in tetrahydrofuran T=-78°C; 2: With sulfur in tetrahydrofuran T=-33°C; 0.5 h; 3: methyl iodide in tetrahydrofuran T=20°C; 3 h;
参考文献
Stankiewicz, Marek; Nycz, Jacek; Rachon, Janusz
Heteroatom Chemistry, 2002 , vol. 13, # 4 p. 330 - 339
反应条件
in chloroform T=20°C; 48 h;
参考文献
Zaslona, Alexander T.; Hall, C. Dennis
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 3059 - 3064
反应条件
in diethyl ether T=0°C; 0.25 h;
参考文献
Corkins, H. G.; Storace, L.; Weinberger, D.; Osgood, E.; Lowery, S.
Phosphorus and Sulfur and the Related Elements, 1981 , vol. 10, p. 133 - 138
参考文献
Zimin, M. G.; Kamalov, R. M.; Cherkasov, R. A.; Pudovik, A. N.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 371 - 378
反应条件
triethylamine; benzene
参考文献
Mel'nikov,N.N. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1960 , vol. 30, p. 200 - 203,213 - 216
参考文献
Mahajna, Mahmoud; Quistad, Gary B.; Casida, John E.
Chemical Research in Toxicology, 1996 , vol. 9, # 7 p. 1202 - 1206
反应条件
in benzene T=80 - 95°C; 15 h; Title compound not separated from byproducts;
参考文献
Khusainova, N. G.; Sippel', I. Ya.; Berdnikov, E. A.; Cherkasov, R. A.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1985 , vol. 55, # 12 p. 2674 - 2681,2377 - 2383
参考文献
Yamasaki
Bl.Res.Inst.Min.Dressing Met.Chem.Abstr., 1952 , vol. 8, p. 213,215
Bl.Res.Inst.Min.Dressing Met.Chem.Abstr., 1955 , p. 8094
参考文献
Yamasaki
Bl.Res.Inst.Min.Dressing Met.Chem.Abstr., 1952 , vol. 8, p. 213,215
Bl.Res.Inst.Min.Dressing Met.Chem.Abstr., 1955 , p. 8094
反应条件
in chloroform Ambient temperature;
参考文献
Borthakur, R. C.; Goswami, A.; Goswami, M.; Borthakur, N.; Rastogi, R. C.; Bhattacharya, P. R.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 668 - 671
