5-丁基-5-甲基四氢呋喃-2-酮合成路线 （共 12 条）
反应条件
gold(III) chloride; water in toluene T=20°C; 15 h; regioselective reaction;
参考文献
Reddy, Maddi Sridhar; Kumar, Yalla Kiran; Thirupathi, Nuligonda
Organic Letters, 2012 , vol. 14, # 3 p. 824 - 827
反应条件
in diethyl ether; benzene T=-5 - 0°C; 0.25 h;
参考文献
Jung, Michael E.; Yoo, Dongwon
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8565 - 8568
反应条件
disodium hydrogenphosphate; sodium amalgam in methanol T=-10°C; 0.5 h;
参考文献
Carretero, Juan Carlos; Lombaert, Stephane De; Ghosez, Leon
Tetrahedron Letters, 1987 , vol. 28, # 19 p. 2135 - 2138
反应条件
pyridine; xanthone powder; bis(2,4-acetylacetonate)cobalt(II); hydrogen in tetrahydrofuran P=760 Torr; Ambient temperatureIrradiation;
参考文献
Chow, Yuan L.; Huang, Yu-Jin; Dragojlovic, Veljko
Canadian Journal of Chemistry, 1995 , vol. 73, # 5 p. 740 - 742
反应条件
(.eta.5-C5H5)2Sm; oxonium in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Namy, J. L.; Collin, J.; Zhang, J.; Kagan, H. B.
Journal of Organometallic Chemistry, 1987 , vol. 328, p. 81 - 86
反应条件
1: 1) n-BuLi, 2) p-TsOH / 1) THF-hexane, -78 to -45 deg C, 1 h, 2) ClCH2CH2Cl, 50 deg C 2: 74 percent / Na(Hg), Na2HPO4 / methanol / 0.5 h / -10 °C View Scheme
参考文献
Reddy, Maddi Sridhar; Kumar, Yalla Kiran; Thirupathi, Nuligonda
Organic Letters, 2012 , vol. 14, # 3 p. 824 - 827
反应条件
1: N-bromosuccinmide; silver nitrate / acetone / 20 °C 2: gold(III) chloride; water / toluene / 15 h / 20 °C View Scheme
参考文献
Reddy, Maddi Sridhar; Kumar, Yalla Kiran; Thirupathi, Nuligonda
Organic Letters, 2012 , vol. 14, # 3 p. 824 - 827
反应条件
hydrogenchloride; beauverolide Ka T=100°C; 72 h;
参考文献
Grove, John Frederick
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2878 - 2880
反应条件
1: 1.) tetrabutylammonium fluoride, water / 1.) THF, 15-30 min, 2.) CH2Cl2 2: triethylamine View Scheme
参考文献
Davies, D. Huw; Hall, Jonathan; Smith, Edward H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 837 - 838
反应条件
hydrogenchloride; beauverolide Ka; D-amino-acid oxidase; sodium pyrophosphate buffer 1.) 110 deg C, 3 d, 2.) 38 deg C, 1 h; Multistep reaction;
参考文献
Grove, John Frederick
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2878 - 2880
