1-特-丁基-4-硝基苯合成路线 (共 81 条)
反应条件
sulfuric acid; nitric acid T=-50°C; 2 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 42, # 1 p. 87 - 99
反应条件
1: 74 percent / N,N-dimethylaniline / diethyl ether / 2 h / Heating 2: 18 percent / acetyl nitrate / acetic anhydride / 2 h / -30 - -10 °C View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 42, # 1 p. 87 - 99
反应条件
trinitratooxovanadium(V) in dichloromethane 0.05 h; Ambient temperature;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 10 p. 1589 - 1590
反应条件
oxygen; sodium 1) THF, 23 gradC; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, p. 701 - 708
Zhurnal Organicheskoi Khimii, , vol. 22, # 4 p. 785 - 794
反应条件
4-Nitrobenzenediazonium tetrafluoroborate; magnesium 1.) THF, reflux, 2.) THF, 30 deg C, 90 s; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 23, # 51 p. 5475 - 5478
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2079,2083
Journal of the Chemical Society, , p. 1890
反应条件
magnesium 1.) THF, reflux, 2.) THF, 30 deg C, 90 s; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 23, # 51 p. 5475 - 5478
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2079,2083
Journal of the Chemical Society, , p. 1890
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2079,2083
Journal of the Chemical Society, , p. 1890
反应条件
nitric acid T=-50°C; 1 h; other temperatures; further nitration agents; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 46, # 11 p. 2376 - 2379