2’’-溴-[1,1’:4’,1’’]三联苯基合成路线 (共 5 条)
反应条件
1: acetic acid; acetic acid anhydride; nitrogen oxide View Scheme
参考文献
Journal of the Chemical Society, , p. 1364,1371
Journal of the Chemical Society, , p. 369,371
参考文献
Journal of the Chemical Society, , p. 1364,1371
Journal of the Chemical Society, , p. 369,371
参考文献
Journal of the Chemical Society, , p. 1364,1371
Journal of the Chemical Society, , p. 369,371
参考文献
Journal of the Chemical Society, , p. 1364,1371
Journal of the Chemical Society, , p. 369,371
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / |Inert atmosphere
1.2: 12 h / 23 °C / |Inert atmosphere
2.1: [Au(1,3-bis(2,6-di-isopropylphenyl)imidazol-2-ylidene)(NCPh)]+SbF6- / 1,2-dichloro-ethane / 3 h / 120 °C / |Sealed tube; |Inert atmosphere
View Scheme
参考文献
Wang, Yahui; McGonigal, Paul R.; Herle, Bart; Besora, Maria; Echavarren, Antonio M.
Journal of the American Chemical Society, 2014 , vol. 136, # 2 p. 801 - 809