4,4'二硝基-对三联苯合成路线 （共 30 条）
反应条件
Pd black; potassium carbonate in methanol; acetonitrile T=20°C; Suzuki Coupling; 2 h;
参考文献
Catalysis Communications, , vol. 31, p. 16 - 20
反应条件
silver carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Suzuki cross-coupling reaction; 16 h; Heating;
参考文献
Synthesis, , # 6 p. 757 - 760
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethylene glycol dimethyl ether T=80°C; 16 h;
参考文献
Tetrahedron Letters, , vol. 38, # 38 p. 6781 - 6784
反应条件
nitric acid; acetic acid
参考文献
Chemische Berichte, , vol. 72, p. 2026
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium carbonate in tetrahydrofuran; water T=50°C; Suzuki-Miyaura cross-coupling reaction; 24 h; Inert atmosphere;
参考文献
Synlett, , # 12 p. 1761 - 1765
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in tetrahydrofuran 48 h; RefluxInert atmosphere;
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 8 p. 1881 - 1884
反应条件
tetrakis(triphenylphosphine) palladium(0); caesium carbonate in methanol; toluene Suzuki-Miyaura coupling; Heating;
参考文献
Journal of Organic Chemistry, , vol. 70, # 9 p. 3730 - 3733
反应条件
tetrakis(triphenylphosphine) palladium(0); silver carbonate in tetrahydrofuran Suzuki-Miyaura coupling; Heating;
参考文献
Journal of Organic Chemistry, , vol. 70, # 9 p. 3730 - 3733
反应条件
nitric acid; acetic acid T=100°C;
参考文献
Journal of the Chemical Society, , p. 1364,1371
Journal of the Chemical Society, , p. 369,371
反应条件
1: KHF2 / methanol; water / 20 °C 2: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; potassium carbonate / tetrahydrofuran; water / 24 h / 50 °C / Inert atmosphere View Scheme
参考文献
Synlett, , # 12 p. 1761 - 1765
