1,1,3,3-四甲基二硅氧烷合成路线 (共 158 条)
反应条件
trimethylsilyl trifluoromethanesulfonate 24 h;
参考文献
Procter, Ian; Azouani, Sobine Isabelle; Houbrichs, Rolf
Patent: US2007/249502 A1, 2007 ;
Location in patent: Page/Page column 17 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 23.3333 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-9 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.00722222 - 1.72222 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-9 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.00583333 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-10 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.0213889 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-10 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.0444444 - 13.8889 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-10 ;
反应条件
nickel T=20°C; Further byproducts given;
参考文献
Voronkov; Basenko; Gebel'; Chuvashev
Doklady Chemistry, 2003 , vol. 393, # 4-6 p. 289 - 291
参考文献
De Vekki; Skvortsov
Russian Journal of General Chemistry, 2009 , vol. 79, # 4 p. 762 - 777
反应条件
iodine Oxidation; Heating;
参考文献
Rakhlin; Turkin; Mirskov; Voronkov
Doklady Chemistry, 1999 , vol. 367, # 1-3 p. 176 - 179
反应条件
hydroquinone in neat (no solvent) mixt., contg. hydroquinone (polymerization inhibitor), kept 30 days at 20°C; pptn., liquid phase sepd. (decantation), crystals washed (cold hexane);
参考文献
Mironov, V. F.; Nuridzhanyan, A. K.; Feoktistov, A. E.
Journal of General Chemistry USSR (English Translation), 1990 , vol. 60, p. 125 - 127
Zhurnal Obshchei Khimii, 1990 , vol. 60, p. 143 - 146