1,1,3,3-四甲基二硅氧烷 合成路线 (共 158 条)
反应条件
hydroquinone in neat (no solvent) mixt., kept 13 days in presence of hydroquinone as polymerization inhibitor, 20°C; pptn., liquid phase sepd. by decantantion, crystals washed (hexane),;
参考文献
Mironov, V. F.; Nuridzhanyan, A. K.; Feoktistov, A. E.
Journal of General Chemistry USSR (English Translation), 1990 , vol. 60, p. 125 - 127
Zhurnal Obshchei Khimii, 1990 , vol. 60, p. 143 - 146
反应条件
Halloysite supported platinum catalyst T=60°C; 10 h;
参考文献
Zhang, Daohong; Liang, Enbin; Li, Tingcheng; Chen, Sufang; Zhang, Junheng; Cheng, Xinjian; Zhou, Jiliang; Zhang, Aiqing
RSC Advances, 2013 , vol. 3, # 9 p. 3095 - 3102
反应条件
cis-[Pt(BnS)2Cl2] in dichloromethane; toluene T=80 - 100°C; Sealed tube;
参考文献
Il'Ina; De Vekki; Skvortsov
Russian Journal of General Chemistry, 2014 , vol. 84, # 1 p. 40 - 69
Zh. Obshch. Khim., 2014 , vol. 84, # 1 p. 43 - 73,31
反应条件
carbene divinyltetramethyldisiloxane platinum T=100 - 120°C; Inert atmosphere;
参考文献
Gelest Technologies Inc.
Patent: US2010/280266 A1, 2010 ;
Location in patent: Page/Page column 3 ;
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反应条件
18547-30-3 2,2,7,7,9,9,14,14-八甲基-3,8,13-三氧杂-2,7,9,14-四硅杂十五烷
反应条件
platinum (IV)-chloride in isopropyl alcohol T=80 - 120°C; 2.5 h;
参考文献
Pusztai, Erika; Nagy, Jozsef; Wagner, Oedoen
Main Group Metal Chemistry, 2012 , vol. 35, # 3-4 p. 91 - 97
反应条件
dihydrogen hexachloroplatinate
参考文献
Bank,H.M. et al.
Journal of Organic Chemistry, 1964 , vol. 29, p. 792 - 794
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.0213889 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-10 ;
反应条件
tris(pentafluorophenyl)-borane in N-dodecane; toluene T=20°C; 0.0444444 - 13.8889 h; Product distribution / selectivity;
参考文献
GENERAL ELECTRIC COMPANY
Patent: WO2006/115788 A2, 2006 ;
Location in patent: Page/Page column 8-10 ;
参考文献
Zhdanov,A.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1973 , vol. 43, p. 1274 - 1279,1265 - 1269
参考文献
De Vekki; Skvortsov
Russian Journal of General Chemistry, 2009 , vol. 79, # 4 p. 762 - 777