1,1,3,3-四甲基二硅氧烷合成路线 （共 158 条）
反应条件
di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium; biphenyl in deuterated toluene
T=40°C; 3 h; Sealed tubeInert atmosphere;
参考文献
Igarashi, Masayasu; Matsumoto, Tomohiro; Kobayashi, Toshiaki; Sato, Kazuhiko; Ando, Wataru; Shimada, Shigeru; Hara, Masanao; Uchida, Hiroshi
Journal of Organometallic Chemistry, 2014 , vol. 752, p. 141 - 146
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107-50-62,2,4,4,6,6,8,8,10,10,12,12,14,14-十四甲基-1,3,5,7,9,11,13-七氧杂-2,4,6,8,10,12,14-七硅杂环十四烷+
参考文献
Basenko; Klyba; Voronkov
Russian Journal of General Chemistry, 2000 , vol. 70, # 9 p. 1368 - 1370
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in toluene
T=45°C; 24 h;
参考文献
Jankowiak, Marcin; MacIejewski, Hieronim; Gulinski, Jacek
Journal of Organometallic Chemistry, 2005 , vol. 690, # 20 SPEC. ISS. p. 4478 - 4487
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in toluene
T=45°C; 24 h; Product distribution; Further Variations:Temperatures;
参考文献
Jankowiak, Marcin; MacIejewski, Hieronim; Gulinski, Jacek
Journal of Organometallic Chemistry, 2005 , vol. 690, # 20 SPEC. ISS. p. 4478 - 4487
反应条件
1: With methanol; sulfuric acid
T=5 - 10°C; 0.75 h;
2: With water
T=5 - 25°C; 3.5 h; Product distribution / selectivity;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: EP1510520 A1, 2005 ;
Location in patent: Page/Page column 16 ;
参考文献
Mironov,V.F. et al.
Doklady Chemistry, 1975 , vol. 224, p. 564 - 567
Dokl. Akad. Nauk SSSR Ser. Khim., 1975 , vol. 224, p. 600 - 603
反应条件
phosphorus pentachloride in tetrachloromethane
24 h; Heating;
参考文献
Jankowiak, Marcin; MacIejewski, Hieronim; Gulinski, Jacek
Journal of Organometallic Chemistry, 2005 , vol. 690, # 20 SPEC. ISS. p. 4478 - 4487
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in toluene
Heating;
参考文献
Jankowiak, Marcin; MacIejewski, Hieronim; Gulinski, Jacek
Journal of Organometallic Chemistry, 2005 , vol. 690, # 20 SPEC. ISS. p. 4478 - 4487
