1,1,3,3-四甲基二硅氧烷合成路线 （共 158 条）
反应条件
gold(III) chloride in 1,2-dichloro-ethane 5 h; Reflux;
参考文献
Lykakis, Ioannis N.; Psyllaki, Androniki; Stratakis, Manolis
Journal of the American Chemical Society, 2011 , vol. 133, # 27 p. 10426 - 10429
反应条件
1: orthosilicic acid tetramethyl ester With hydrogenchloride; methanol; water T=5 - 10°C; 2: 1,1,3,3-tetramethyldisiloxane T=5 - 10°C; 4 h; 3: With sulfuric acid; water more than 3 stages;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: EP1510520 A1, 2005 ;
Location in patent: Page/Page column 16 ;
反应条件
hydrogenchloride in water; toluene T=47°C; 1 h; Inert atmosphere;
参考文献
MOMENTIVE PERFORMANCE MATERIALS GMBH
Patent: US2012/46485 A1, 2012 ;
Location in patent: Page/Page column 5 ;
反应条件
trichloroisocyanuric acid in dichloromethane Heating;
参考文献
Journal of Organometallic Chemistry, , vol. 692, # 10 p. 1892 - 1897
反应条件
phosphorus pentachloride in tetrachloromethane 24 h; Heating;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 20 SPEC. ISS. p. 4478 - 4487
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in toluene Heating;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 20 SPEC. ISS. p. 4478 - 4487
反应条件
iodine 0.166667 h; Heating;
参考文献
Voronkov, M. G.; Turkin, Yu. A.; Mirskov, R. G.; Kuz'mina, E. E.; Rakhlin, V. I.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 11 p. 2641,2362
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) T=95 - 125°C; Inert atmosphere;
参考文献
Niu, Yuzhong; Lu, Haifeng; Wang, Dengxu; Yue, Yuanzhi; Feng, Shengyu
Journal of Organometallic Chemistry, 2011 , vol. 696, # 2 p. 544 - 550
反应条件
dihydrogen hexachloroplatinate; ethanol
参考文献
Saam; Speier
Journal of Organic Chemistry, 1959 , vol. 24, p. 119
反应条件
Pd0(tris(tert-butyl)phosphine)2; N-ethyl-N,N-diisopropylamine in tetrahydrofuran T=20°C; 4 h;
参考文献
Kurihara, Yu; Yamanoi, Yoshinori; Nishihara, Hiroshi
Chemical Communications, 2013 , vol. 49, # 96 p. 11275 - 11277
