1,1,3,3-四甲基二硅氧烷合成路线 (共 158 条)
参考文献
Wacker-Chemie GmbH
Patent: US6284907 B1, 2001 ;
反应条件
water; diisopropylamine in DMF-d7 T=-78°C; Substitution; Mannich-type reaction; Addition; 18 h; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 39, # 11 p. 1958 - 1960
反应条件
in dichloromethane; 4-(dicyanomethylene)-2-methyl-6-(4-dimethylaminostyryl)-4H-pyran
参考文献
US6342349 B1, ;
US6200755 B1, ;
反应条件
water in benzene T=38 - 40°C; 2 h;
参考文献
Applied Organometallic Chemistry, , vol. 24, # 3 p. 251 - 256
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <4>9, p. 63,67,70
Bulletin of the Chemical Society of Japan, , vol. 29, p. 236,238,240
Journal of the American Chemical Society, , vol. 79, p. 974,976
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 265 - 270
反应条件
water in tetrahydrofuran 0.5 h; Cooling with ice;
参考文献
Kawahara, Kazufumi; Hagiwara, Yoshiaki; Kuroda, Kazuyuki
Chemistry - A European Journal, 2011 , vol. 17, # 47 p. 13188 - 13196
反应条件
trichlorosilane Hydrolysis;
参考文献
Journal of the American Chemical Society, , vol. 79, p. 974,976
反应条件
T=740°C; P=0.0005 Torr; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 28, # 51 p. 6421 - 6424
反应条件
lithium perchlorate in tetrahydrofuran Electrolysis;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 1-2 p. 105 - 110
反应条件
in benzene T=26.9°C; Equilibrium constant;
参考文献
Journal of the American Chemical Society, , vol. 113, # 15 p. 5581 - 5583