(5α,17β)-17-甲基-2-雄烯-3,17-二醇合成路线 （共 4 条）
反应条件
in tetrahydrofuran T=0 - 20°C; Inert atmosphere;
参考文献
UNIVERSITE LAVAL; POIRIER, Donald; ROY, Jenny; MALTAIS, Rene
Patent: WO2010/60215 A1, 2010 ;
Location in patent: Page/Page column 54; 93 ;
反应条件
1: (i) NaBH4, EtOH, (ii) Zn, AcOH, (iii) NaOH, MeOH 2: CrO3, H2SO4 / acetone 3: diethyl ether; benzene View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 6, p. 156 - 161
反应条件
1: CrO3, H2SO4 / acetone 2: diethyl ether; benzene View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 6, p. 156 - 161
反应条件
1: (i) B2H6, THF, (ii) aq. H2O2, NaOH 2: CrO3, aq. H2SO4 / acetone View Scheme
参考文献
Cross,A.D. et al.
Journal of Medicinal and Pharmaceutical Chemistry, 1962 , vol. 5, p. 406 - 408
