2-甲氧基蒽-9,10-二酮合成路线 （共 50 条）
反应条件
oxygen; copper diacetate; silver carbonate in N,N-dimethyl-formamide T=140°C; P=760.051 Torr; 36 h;
参考文献
Bhadra, Sukalyan; Dzik, Wojciech I.; Goossen, Lukas J.
Synthesis (Germany), 2013 , vol. 45, # 17 art. no. SS-2013-Z0414-PSP, p. 2387 - 2390
反应条件
tert.-butylhydroperoxide; PhCl(PPh3)3 in benzene T=70°C; 36 h; Var. cat.: VO(acac)2;
参考文献
Mueller, Paul; Bobillier, Christiane
Tetrahedron Letters, 1983 , vol. 24, # 49 p. 5499 - 5500
反应条件
sodium hydroxide; dihydrogen peroxide in ethanol a) 5 h, 75 deg C, b) 12 h, room temp.;
参考文献
Bhawal, Baburao M.; Khanapure, Subhash P.; Zhang, Hongming; Biehl, Edward R.
Journal of Organic Chemistry, 1991 , vol. 56, # 8 p. 2846 - 2849
反应条件
sodium hydride in tert-butyl methyl ether; N,N-dimethyl-formamide T=20°C; 20 h;
参考文献
Saha, Koushik; Lam, Kok Wai; Abas, Faridah; Sazali Hamzah; Stanslas, Johnson; Hui, Lim Siang; Lajis, Nordin H.
Medicinal Chemistry Research, 2013 , vol. 22, # 5 p. 2093 - 2104
反应条件
sodium methylate 72 h; Heating;
参考文献
Khenkin; Weiner; Wang; Neumann
Journal of the American Chemical Society, 2001 , vol. 123, # 35 p. 8531 - 8542
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in diethyl ether 1.) -78 deg C, 1 h, 2.) -78 deg C -> RT, 12 h;
参考文献
Watanabe; Snieckus
Journal of the American Chemical Society, 1980 , vol. 102, # 4 p. 1457 - 1460
反应条件
aluminium trichloride in nitrobenzene T=100°C; 5 h;
参考文献
Sartori, Giovanni; Casnati, Giuseppe; Bigi, Franca; Foglio, Federica
Gazzetta Chimica Italiana, 1990 , vol. 120, # 1 p. 13 - 19
反应条件
diphosphoric acid tetrachloride T=40°C; 2 h;
参考文献
El-Sayrafi, Sami; Rayyan, Saleh
Molecules, 2001 , vol. 6, # 3 p. 279 - 286
反应条件
1H-imidazole; oxygen in ethanol 25 h; Ambient temperature;
参考文献
Iwata, Masaaki; Kuzuhara, Hiroyoshi
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 5 p. 1609 - 1610
参考文献
Brisson, Clement; Brassard, Paul
Journal of Organic Chemistry, 1981 , vol. 46, # 9 p. 1810 - 1814
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Lu, Lingang; Chen, Qiyin; Zhu, Xiaozhang; Chen, Chuanfeng
Synthesis, 2003 , # 16 p. 2464 - 2466
