3-偶氮基-1H-吲哚-2-醇合成路线 （共 7 条）
反应条件
1: With benzoic acid; hydrazine in tetrahydrofuran T=20°C; 16 h; 2: With N-iodo-N-potassio-p-toluenesulphonamide; potassium hydroxide in tetrahydrofuran; water T=20°C;
参考文献
Nicolle, Simon M.; Moody, Christopher J.
Chemistry - A European Journal, 2014 , vol. 20, # 15 p. 4420 - 4425
反应条件
sodium hydroxide T=20 - 60°C; 3 h;
参考文献
Varano, Flavia; Catarzi, Daniela; Colotta, Vittoria; Calabri, Francesca Romana; Lenzi, Ombretta; Filacchioni, Guido; Galli, Alessandro; Costagli, Chiara; Deflorian, Francesca; Moro, Stefano
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 19 p. 5536 - 5549
反应条件
4-Acetylaminobenzenesulfonyl Azide; triethylamine in acetonitrile 12 h; Ambient temperature;
参考文献
Baum, Jonathan S.; Shook, David A.; Daries, Huw M. L.; Smith, H. David
Synthetic Communications, 1987 , vol. 17, # 14 p. 1709 - 1716
反应条件
ammonium hydroxide; copper(l) chloride in dimethyl sulfoxide 0.0833333 h;
参考文献
Muzalevskiy; Balenkova; Shastin; Magerramov; Shikhaliev; Nenajdenko
Russian Chemical Bulletin, 2011 , vol. 60, # 11 p. 2343 - 2346
参考文献
Tacconi, G.; Righetti, P. P.; Desimoni, G.
Journal fuer Praktische Chemie (Leipzig), 1980 , vol. 322, # 4 p. 679 - 684
反应条件
hydrogenchloride in water
T=30°C; 0.5 h; Inert atmosphere;
参考文献
Bergman, Jan; Stensland, Birgitta
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 1 p. 1 - 10
反应条件
1: 75 percent / toluene / Heating
2: 90 percent / KOH / ethanol / 1 h / 100 °C
View Scheme
参考文献
Varano, Flavia; Catarzi, Daniela; Colotta, Vittoria; Calabri, Francesca Romana; Lenzi, Ombretta; Filacchioni, Guido; Galli, Alessandro; Costagli, Chiara; Deflorian, Francesca; Moro, Stefano
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 19 p. 5536 - 5549
