copper(II) bis(trifluoromethanesulfonate); urea in ethyl acetate T=60°C; Chan-Lam reaction; 24 h;

暂无反应条件数据

quinoline; copper

1: pyridine 2: quinoline; copper-powder View Scheme

diethyl ether

暂无反应条件数据

1: 1.) N-chlorosuccinimide, 2.) KHCO3, water / 1.) AcOEt, 65 deg C, 0.5 h, 2.) 25 deg C, 24 h 2: 64 percent / sodium acetate, KF / acetic acid / 2 h / Heating 3: 75 percent / NaOH / methanol / 24 h 4: H2, boric acid / Raney-Ni / methanol; H2O / 1 h / Heating 5: aq. NaOH / 1 h / Heating View Scheme

1: 1.) N-chlorosuccinimide, 2.) KHCO3, water / 1.) AcOEt, 65 deg C, 0.5 h, 2.) 25 deg C, 24 h 2: 64 percent / sodium acetate, KF / acetic acid / 2 h / Heating 3: 75 percent / NaOH / methanol / 24 h 4: H2, boric acid / Raney-Ni / methanol; H2O / 1 h / Heating View Scheme

potassium hydroxide