1-苯基-4-戊烯-1-酮合成路线 （共 116 条）
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; acetonitrile
3 h; Irradiation;
参考文献
Piva, Olivier; Amougay, Aicha; Pete, Jean-Pierre
Tetrahedron Letters, 1991 , vol. 32, # 32 p. 3993 - 3996
反应条件
1,2-bis-(diphenylphosphino)ethane; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
3 h; Ambient temperaturevar.: solvent(THF), time, catalyst;
参考文献
Inoue, Yoshio; Toyofuku, Masanori; Hashimoto, Harukichi
Chemistry Letters, 1984 , p. 1227 - 1228
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide; diethyl ether
1.5 h; -78 deg C -> r.t.; Title compound not separated from byproducts;
参考文献
Vaughan, William S.; Gu, Henry H.; McDaniel, Keith F.
Tetrahedron Letters, 1997 , vol. 38, # 11 p. 1885 - 1888
反应条件
palladium diacetate; sodium carbonate; triphenylphosphine in tetrahydrofuran
T=120°C; P=15001.5 Torr; Inert atmosphereAutoclave;
参考文献
Pirez, Cyril; Dheur, Julien; Sauthier, Mathieu; Castanet, Yves; Mortreux, Andre
Synlett, 2009 , # 11 p. 1745 - 1748
反应条件
1: With (1-butene)ZrCp2 in tetrahydrofuran; hexane
T=-78 - 20°C; 25 h;
2: With water in tetrahydrofuran; hexane
参考文献
Kitamura, Mitsuru; Shintaku, Yuki; Kudo, Daisuke; Okauchi, Tatsuo
Tetrahedron Letters, 2010 , vol. 51, # 37 p. 4890 - 4893
反应条件
tris-(dibenzylideneacetone)dipalladium(0); bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate in toluene
T=80°C; 3 h; Inert atmosphere;
参考文献
Nicolai, Stefano; Sedigh-Zadeh, Raha; Waser, Jeroime
Journal of Organic Chemistry, 2013 , vol. 78, # 8 p. 3783 - 3801
反应条件
titanium tetrachloride in dichloromethane
T=-78°C;
参考文献
Sakurai,H. et al.
Tetrahedron Letters, 1977 , p. 4045 - 4048
反应条件
iodosylbenzene; boron trifluoride diethyl etherate; dicyclohexyl-carbodiimide in dichloromethane
5 h; Ambient temperature;
参考文献
Ochiai, Masahito; Ukita, Tatsuzo; Nagao, Yoshimitsu; Fujita, Eiichi
Journal of the Chemical Society, Chemical Communications, 1984 , # 15 p. 1007 - 1008
反应条件
in benzene
0.333333 h; Irradiation;
参考文献
Toru; Watanabe; Tsusaka; Gautam; Tazawa; Bakouetila; Yoneda; Ueno
Tetrahedron Letters, 1992 , vol. 33, # 28 p. 4037 - 4040
反应条件
nickel; acetic acid in n-heptane
参考文献
Boivin, Jean; Schiano, Anne-Marie; Zard, Samir Z.; Zhang, Haiwen
Tetrahedron Letters, 1999 , vol. 40, # 24 p. 4531 - 4534
