1-苯基-4-戊烯-1-酮合成路线 （共 116 条）
反应条件
lithium boron tetrafluoride; [Ru(2,2′-bipyridine)3][hexafluorophosphate]2; N-ethyl-N,N-diisopropylamine in hexadeuterioacetone
T=23°C; 0.666667 h; Inert atmosphereIrradiation;
参考文献
Zlotorzynska, Maria; Sammis, Glenn M.
Organic Letters, 2011 , vol. 13, # 23 p. 6264 - 6267
反应条件
1: 1.) LDA / 1.) THF, 0 deg C, 2 h, 2.) THF, 0 deg C -> room temperature; room temperature, 2 h
2: 85 percent / Amberlyst / acetone / 18 h / Ambient temperature
View Scheme
参考文献
Crotti, Paolo; Di Bussolo, Valeria; Favero, Lucilla; Macchia, Franco; Pineschi, Mauro; Napolitano, Elio
Tetrahedron, 1999 , vol. 55, # 18 p. 5853 - 5866
反应条件
lithium aluminium tetrahydride; Cp2Ni in tetrahydrofuran
16 h; Ambient temperature;
参考文献
Chan, Man-Chor; Cheng, Kwok-Man; Ho, Kim Man; Ng, Chi Tat; Yam, Tsz Man; et al.
Journal of Organic Chemistry, 1988 , vol. 53, # 19 p. 4466 - 4471
反应条件
tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
Ambient temperaturefurther solvent;
参考文献
Tsuda, Tetsuo; Chujo, Yoshiki; Nishi, Sei-ichi; Tawara, Kunio; Saegusa, Takeo
Journal of the American Chemical Society, 1980 , vol. 102, # 20 p. 6381 - 6384
反应条件
air; sodium hydride; p-toluenesulfinic acid sodium salt in tetrachloromethane
Ambient temperature;
参考文献
Miyashi, Tsutomu; Kamata, Masaki; Nishizawa, Yoshinori; Mukai, Toshio
Journal of the Chemical Society, Chemical Communications, 1984 , # 3 p. 147 - 148
反应条件
samarium; mercury dichloride in tetrahydrofuran; water
T=20°C; Desulfonylation;
参考文献
Guo, Hongyun; Zhang, Yongmin
Synthetic Communications, 2000 , vol. 30, # 14 p. 2559 - 2564
反应条件
1: With titanium tetrachloride in dichloromethane
0.5 h;
2: With chloro-trimethyl-silane in dichloromethane
T=-78°C;
参考文献
Yadav, Veejendra K.; Balamurugan, Rengarajan
Organic Letters, 2003 , vol. 5, # 23 p. 4281 - 4284
反应条件
1: With (1-butene)ZrCp2 in tetrahydrofuran; hexane
T=-78 - 20°C; 7 h;
2: With water in tetrahydrofuran; hexane
参考文献
Kitamura, Mitsuru; Shintaku, Yuki; Kudo, Daisuke; Okauchi, Tatsuo
Tetrahedron Letters, 2010 , vol. 51, # 37 p. 4890 - 4893
反应条件
water in ethylene glycol dimethyl ether
T=84°C; 20 h;
参考文献
Vallee, Yannick; Worrell, Mark
Journal of the Chemical Society, Chemical Communications, 1992 , # 22 p. 1680 - 1681
反应条件
sodium hydroxide in ethanol
1.5 h; Heating;
参考文献
Fox, David J.; Pedersen, Daniel Sejer; Warren, Stuart
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 16 p. 3102 - 3107
