2,4,6-环庚三烯-1-甲酰氯合成路线 （共 10 条）
反应条件
1: 64 percent / NaHCO3 / methanol; H2O / 2 h / Heating 2: thionyl chloride View Scheme
参考文献
Facchetti, Antonio; Streitwieser, Andrew
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2281 - 2286
反应条件
1: 46.3 percent / conc. H2SO4 / 35 h / Heating 2: 74 percent / HaHCO3, H2O / methanol / 2 h / Heating 3: SOCl2 / 42 h / Ambient temperature View Scheme
参考文献
Facchetti, Antonio; Streitwieser, Andrew
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2281 - 2286
参考文献
Tidwell, Thomas T.; Fenwick, Michael H.
European Journal of Organic Chemistry, 2001 , # 18 p. 3415 - 3419
参考文献
Tetrahedron Letters, , vol. 26, # 10 p. 1289 - 1292
参考文献
Tetrahedron Letters, , vol. 26, # 10 p. 1289 - 1292
反应条件
nitromethane; silver perchlorate T=85 - 90°C;
参考文献
Dewar; Ganellin
Journal of the Chemical Society, 1959 , p. 2438,2440
参考文献
Ruechardt,C.; Schwarzer,H.
Chemische Berichte, 1966 , vol. 99, p. 1861 - 1870
参考文献
Facchetti, Antonio; Streitwieser, Andrew
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2281 - 2286
反应条件
1: (i) Et2O, (ii) CuSO4, hexane, benzene
2: diethyl ether; methanol
View Scheme
参考文献
Doering,W. von E. et al.
Tetrahedron, 1967 , vol. 23, p. 3943 - 3963
反应条件
1: (i) Et2O, (ii) CuSO4, hexane, benzene
2: diethyl ether
View Scheme
参考文献
Doering,W. von E. et al.
Tetrahedron, 1967 , vol. 23, p. 3943 - 3963
