2,3,4,6-四甲基苯酚合成路线 (共 38 条)
反应条件
water; basic magnesium carbonate; magnesium oxide; manganese oxalate; mixture of, calcined at 370 degrees C T=370 - 500°C; P=760.051 Torr; 359 - 596 h; Product distribution / selectivity;
参考文献
Honshu Chemical Industry Co., Ltd.
Patent: US6951966 B1, 2005 ;
Location in patent: Page/Page column 9-10 ;
反应条件
1: 92 percent / NaBr; acetic acid; H2SO4 / 1 h / 20 °C 2: 77 percent / LiAlH4 / diethyl ether / 0.5 h / 20 °C View Scheme
参考文献
Nagel, Matthias; Hansen, Hans-Juergen
Helvetica Chimica Acta, 2000 , vol. 83, # 5 p. 1022 - 1048
反应条件
potassium hydroxide; water T=300°C;
参考文献
Raistrick; Ross
Biochemical Journal, 1952 , vol. 50, p. 635,645
反应条件
dihydrogen peroxide in dichloro difluoro methane; epoxysulfonyl fluoride T=-80 - -70°C; 2.5 h; Yield given. Yields of byproduct given;
参考文献
Koptyug, V. A.; Rogozhnikova, O. Yu.; Detsina, A. N.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 7 p. 1193 - 1203
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 7 p. 1345 - 1357
反应条件
CrPb; magnesium oxide T=440°C; P=760 Torr; 2 h;
参考文献
Ke, Jyh-Harng; Zena, Jyh-Myng; Wang, Fey-Long
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 6 p. 1407 - 1410
反应条件
CrPb; magnesium oxide T=440°C; P=760 Torr; 2 h;
参考文献
Ke, Jyh-Harng; Zena, Jyh-Myng; Wang, Fey-Long
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 6 p. 1407 - 1410
反应条件
CrPb; magnesium oxide T=440°C; P=760 Torr; 2 h;
参考文献
Ke, Jyh-Harng; Zena, Jyh-Myng; Wang, Fey-Long
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 6 p. 1407 - 1410
反应条件
CrPb; magnesium oxide T=440°C; P=760 Torr; 2 h;
参考文献
Ke, Jyh-Harng; Zena, Jyh-Myng; Wang, Fey-Long
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 6 p. 1407 - 1410
反应条件
methanol; sodium methylate T=220°C;
参考文献
Burawoy; Chamberlain
Journal of the Chemical Society, 1949 , p. 624
参考文献
Miller,B.
Journal of Organic Chemistry, 1977 , vol. 42, # 8 p. 1402 - 1408