sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in ethanol; dichloromethane T=30°C; 0.416667 h; ultrasound cleaner; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: carbon monoxide With potassium cyanide; Ni(CN)2*4H2O; CoCl2*6H2O; hydrogen; potassium hydroxide in toluene T=95°C; 2 h; 2: 1-(2,2-dibromocyclopropyl)benzene in toluene T=95°C; 48 h; optical yield given as percent de;
参考文献
Cheng, Kejun; Lee, Yong Sok; Rothman, Richard B.; Dersch, Christina M.; Bittman, Ross W.; Jacobson, Arthur E.; Rice, Kenner C.
Journal of Medicinal Chemistry, 2011 , vol. 54, # 4 p. 957 - 969
