4-氯-1-甲基-1H-喹啉-2-酮合成路线 （共 10 条）
反应条件
trichlorophosphate in 1,4-dioxane T=120°C; 0.416667 h; microwave irradiation;
参考文献
Hashim, Jamshed; Glasnov, Toma N.; Kremsner, Jennifer M.; Kappe, C. Oliver
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1707 - 1710
反应条件
potassium hydroxide; potassium hexacyanoferrate(III) in water 1 h; cooling;
参考文献
Hoshino, Masato; Taguchi, Tsuyoshi; Nakano, Hiroto; Tomisawa, Hiroshi; Matsuzaki, Hisao; Fujita, Reiko
Heterocycles, 2007 , vol. 74, # C p. 791 - 802
反应条件
trichlorophosphate und anschliessend mit Phosphor(V)-chlorid;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 1810
反应条件
trichlorophosphate 1 h; Heating;
参考文献
Rao, V. Sudhakar; Darbarwar, Malleshwar
Synthetic Communications, 1989 , vol. 19, # 15 p. 2713 - 2720
反应条件
methanol; sodium hydroxide; water
参考文献
Chemische Berichte, , vol. 20, p. 2012
反应条件
thionyl chloride 2 h; Ambient temperature;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 24, p. 62 - 66
反应条件
sodium azide in N,N-dimethyl-formamide T=80°C; 2 h;
参考文献
Stadlbauer, Wolfgang
Monatshefte fuer Chemie, 1986 , vol. 117, p. 1305 - 1324
反应条件
hydrazine hydrate in N,N-dimethyl-formamide Condensation; 3 h; Heating;
参考文献
Abass, Mohamed
Synthetic Communications, 2000 , vol. 30, # 15 p. 2735 - 2757
反应条件
[2,2']bipyridinyl; potassium iodide; bis(1,5-cyclooctadiene)nickel (0) in 1,4-dioxane T=130°C; Ullmann-type reaction; 0.583333 h; microwave irradiation; Product distribution; Further Variations:CatalystsReagentsSolventsTemperaturestimes; catalyst concentrations; reagent concentrations;
参考文献
Hashim, Jamshed; Kappe, C. Oliver
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 14-15 p. 2353 - 2360
反应条件
triethylamine; triphenylphosphine; palladium diacetate in ethylene glycol dimethyl ether; water
T=150°C; Suzuki cross-coupling; 0.5 h; microwave irradiation;
参考文献
Glasnov, Toma N.; Stadlbauer, Wolfgang; Kappe, C. Oliver
Journal of Organic Chemistry, 2005 , vol. 70, # 10 p. 3864 - 3870
