1-(9H-咔唑-3-基)乙酮合成路线 (共 10 条)
反应条件
Cp*Rh(OTf)2; copper diacetate; potassium carbonate; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane in o-xylene T=130°C; 24 h; Inert atmosphere;
参考文献
Jiang, Qibai; Duan-Mu, Dandan; Zhong, Wei; Chen, Hao; Yan, Hong
Chemistry - A European Journal, 2013 , vol. 19, # 6 p. 1903 - 1907
反应条件
potassium hydroxide in methanol T=70°C; 12 h;
参考文献
St. Jean Jr., David J.; Poon, Steve F.; Schwarzbach, Jamie L.
Organic Letters, 2007 , vol. 9, # 23 p. 4893 - 4896
反应条件
aluminium trichloride; nitrobenzene Erhitzen des Reaktionsgemisches auf 125grad;
参考文献
Plant; Williams
Journal of the Chemical Society, 1934 , p. 1142
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Meitzner
Journal of the American Chemical Society, 1935 , vol. 57, p. 2327
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Plant; Rogers; Williams
Journal of the Chemical Society, 1935 , p. 741,743
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; [bis(acetoxy)iodo]benzene in dichloromethane T=20°C;
参考文献
Khan, Imran A.; Saxena, Anil K.
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 11656 - 11669
反应条件
in cyclohexane T=20°C; 8 h; Irradiation;
参考文献
Zander, Maximilian
Chemische Berichte, 1981 , vol. 114, # 7 p. 2665 - 2667
反应条件
zinc(II) chloride T=150°C; unter Druck;
参考文献
Acheson; Sansom
Journal of the Chemical Society, 1953 , p. 1900
参考文献
Plant; Williams
Journal of the Chemical Society, 1934 , p. 1142
反应条件
hydrogenchloride; amalgamated zinc; methoxybenzene
参考文献
Plant; Williams
Journal of the Chemical Society, 1934 , p. 1142
反应条件
potassium hydroxide; water
参考文献
Plant; Williams
Journal of the Chemical Society, 1934 , p. 1142
反应条件
sodium tetrahydroborate in methanol
T=20°C; 0.5 h;
参考文献
Hu, Qingzhong; Negri, Matthias; Jahn-Hoffmann, Kerstin; Zhuang, Yan; Olgen, Sureyya; Bartels, Marc; Mueller-Vieira, Ursula; Lauterbach, Thomas; Hartmann, Rolf W.
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 16 p. 7715 - 7727