反应条件
1: 0.95 g / POCl3 / 1.5 h / Ambient temperature
2: NH2OH*HCl, NaOH / ethanol; H2O / 0.33 h / Heating
3: Raney Ni alloy, 2 N aq. NaOH / ethanol / 1 h / Ambient temperature
4: 1.) oxygen, tetraphenylporphine, 2.) triphenylphosphine / 1.) CH2Cl2, -70 deg C, irradiation, 2 h, 2.) -70 deg C, 10 min
View Scheme
参考文献
Kuo; Shih
Chemical and Pharmaceutical Bulletin, 1991 , vol. 39, # 1 p. 181 - 183
