alpha-甲基-(3-苄氧基)苄醇合成路线 (共 6 条)
反应条件
lithium aluminium tetrahydride in diethyl ether 1 h;
参考文献
Aggarwal, Rachna; Birkbeck, Anthony A.; Giles, Robin G.F.; Green, Ivan R.; Gruchlik, Yolanta; Oosthuizen, Francois J.
Australian Journal of Chemistry, 2003 , vol. 56, # 5 p. 489 - 498
反应条件
1: 82 percent / potassium carbonate / dimethylformamide / 12 h / Heating 2: 99 percent / lithium aluminium hydride / diethyl ether / 1 h View Scheme
参考文献
Gopalsamy, Ariamala; Kincaid, Scott L.; Ellingboe, John W.; Groeling, Thomas M.; Antrilli, Thomas M.; Krishnamurthy, Girija; Aulabaugh, Ann; Friedrichs, Gregory S.; Crandall, David L.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3477 - 3480
反应条件
1.1: K2CO3 / acetone / Heating 2.1: n-BuLi / -78 °C 2.2: 60 °C View Scheme
参考文献
Gopalsamy, Ariamala; Kincaid, Scott L.; Ellingboe, John W.; Groeling, Thomas M.; Antrilli, Thomas M.; Krishnamurthy, Girija; Aulabaugh, Ann; Friedrichs, Gregory S.; Crandall, David L.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3477 - 3480
反应条件
1: 3-(phenylmethoxy)phenyl bromide With n-butyllithium T=-78°C; 2: acetaldehyde T=60°C;
参考文献
Gopalsamy, Ariamala; Kincaid, Scott L.; Ellingboe, John W.; Groeling, Thomas M.; Antrilli, Thomas M.; Krishnamurthy, Girija; Aulabaugh, Ann; Friedrichs, Gregory S.; Crandall, David L.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3477 - 3480
反应条件
1: 82 percent / potassium carbonate / dimethylformamide / 12 h / Heating 2: 99 percent / lithium aluminium hydride / diethyl ether / 1 h View Scheme
参考文献
Aggarwal, Rachna; Birkbeck, Anthony A.; Giles, Robin G.F.; Green, Ivan R.; Gruchlik, Yolanta; Oosthuizen, Francois J.
Australian Journal of Chemistry, 2003 , vol. 56, # 5 p. 489 - 498
反应条件
jones reagent T=20°C;
参考文献
Gopalsamy, Ariamala; Kincaid, Scott L.; Ellingboe, John W.; Groeling, Thomas M.; Antrilli, Thomas M.; Krishnamurthy, Girija; Aulabaugh, Ann; Friedrichs, Gregory S.; Crandall, David L.
Bioorganic and Medicinal Chemistry Letters, 2004 , vol. 14, # 13 p. 3477 - 3480