2-(二甲氧基甲基)喹喔啉 1,4-二氧化物合成路线 （共 5 条）
参考文献
Burguete, Asuncion; Pontiki, Eleni; Hadjipavlou-Litina, Dimitra; Ancizu, Saioa; Villar, Raquel; Solano, Beatriz; Moreno, Elsa; Torres, Enrique; Perez, Silvia; Aldana, Ignacio; Monge, Antonio
Chemical Biology and Drug Design, 2011 , vol. 77, # 4 p. 255 - 267
反应条件
1: sodium dithionite / water; ethanol / 0.5 h / 20 - 50 °C / |Large scale 2: hydrogenchloride / water / 0.5 h / 50 - 60 °C / |Large scale 3: dihydrogen peroxide; sodium hydroxide / water / 2 h / 17 - 80 °C / |Large scale View Scheme
参考文献
Wong, John W.; Watson Jr., Harry A.; Bouressa, James F.; Burns, Michael P.; Cawley, James J.; Doro, Albert E.; Guzek, Donald B.; Hintz, Michael A.; McCormick, Ellen L.; Scully, Douglas A.; Siderewicz, Joseph M.; Taylor, William J.; Truesdell, Susan J.; Wax, Richard G.
Organic Process Research and Development, 2002 , vol. 6, # 4 p. 477 - 481
反应条件
hydrogenchloride in methanol
参考文献
SPOFA, spojene podniky prop farmaceutickou vyrobu
Patent: US4225604 A1, 1980 ;
反应条件
1: sodium dithionite / water; ethanol / 0.5 h / 20 - 50 °C / |Large scale 2: hydrogenchloride / water / 0.5 h / 50 - 60 °C / |Large scale View Scheme
参考文献
Wong, John W.; Watson Jr., Harry A.; Bouressa, James F.; Burns, Michael P.; Cawley, James J.; Doro, Albert E.; Guzek, Donald B.; Hintz, Michael A.; McCormick, Ellen L.; Scully, Douglas A.; Siderewicz, Joseph M.; Taylor, William J.; Truesdell, Susan J.; Wax, Richard G.
Organic Process Research and Development, 2002 , vol. 6, # 4 p. 477 - 481
反应条件
sodium dithionite in ethanol; water
T=20 - 50°C; 0.5 h; Large scale;
参考文献
Wong, John W.; Watson Jr., Harry A.; Bouressa, James F.; Burns, Michael P.; Cawley, James J.; Doro, Albert E.; Guzek, Donald B.; Hintz, Michael A.; McCormick, Ellen L.; Scully, Douglas A.; Siderewicz, Joseph M.; Taylor, William J.; Truesdell, Susan J.; Wax, Richard G.
Organic Process Research and Development, 2002 , vol. 6, # 4 p. 477 - 481
