1-(3-甲氧基苯基)-吡咯烷合成路线 （共 17 条）
反应条件
sodium t-butanolate; 2-(di-t-butylphosphino)biphenyl palladium in toluene T=80°C; 2.5 h;
参考文献
Zim, Danilo; Buchwald, Stephen L.
Organic Letters, 2003 , vol. 5, # 14 p. 2413 - 2415
反应条件
copper(l) iodide; potassium carbonate; L-proline in dimethyl sulfoxide T=90°C; 31 h;
参考文献
Zhang, Hui; Cai, Qian; Ma, Dawei
Journal of Organic Chemistry, 2005 , vol. 70, # 13 p. 5164 - 5173
反应条件
lithium hexamethyldisilazane; tris(dibenzylideneacetone)dipalladium (0); SIDip*HCl in tetrahydrofuran T=25°C; 20 h;
参考文献
Conesa Lerma, Israel; Cawley, Mark J.; Cloke, F. Geoffrey N.; Arentsen, Katherine; Scott, James S.; Pearson, Stuart E.; Hayler, John; Caddick, Stephen
Journal of Organometallic Chemistry, 2005 , vol. 690, # 24-25 p. 5841 - 5848
反应条件
sodium t-butanolate; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride; chlorobis(triphenylphosphine)(1-naphthyl)nickel(II) in 1,4-dioxane T=110°C; 0.25 h;
参考文献
Gao, Cai-Yan; Yang, Lian-Ming
Journal of Organic Chemistry, 2008 , vol. 73, # 4 p. 1624 - 1627
反应条件
1: With anhydrous copper acetate in tetrahydrofuran; water T=0°C; Sandmeyer type reaction; 14 h; Reflux; 2: With hydrogenchloride in tetrahydrofuran; diethyl ether 3: With sodium hydrogencarbonate in diethyl ether; water
参考文献
Carpenter, Richard D.; Verkman
Organic Letters, 2010 , vol. 12, # 6 p. 1160 - 1163
反应条件
cesium fluoride in acetonitrile T=20°C; 5 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209
反应条件
sodium tetrahydroborate; sulfuric acid; water in tetrahydrofuran; methanol T=10 - 20°C; 1.5 h; Yields of byproduct given;
参考文献
Verardo, Giancarlo; Dolce, Anna; Toniutti, Nicoletta
Synthesis, 1999 , # 1 p. 74 - 79
反应条件
tris-(dibenzylideneacetone)dipalladium(0) in hexane; ethyl acetate; toluene
参考文献
Cytovia, Inc.
Patent: US2003/65018 A1, 2003 ;
反应条件
triethylamine in acetonitrile T=0 - 20°C; Inert atmosphere; Reagent/catalyst;
参考文献
Qian, Xin; Yu, Zailu; Auffrant, Audrey; Gosmini, Corinne
Chemistry - A European Journal, 2013 , vol. 19, # 20 p. 6225 - 6229
反应条件
potassium hydroxide; air; Cd(CH3COO)2*2H2O; ethylene glycol in dimethyl sulfoxide T=85°C; 12 h;
参考文献
Rout, Laxmidhar; Saha, Prasenjit; Jammi, Suribabu; Punniyamurthy, Tharmalingam
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 3 p. 395 - 398
