1,2,4,5-四(三氟甲基)苯合成路线 （共 8 条）
反应条件
sulfur(IV) fluoride T=150°C; 6 h;
参考文献
Dmowski, Wojciech; Porwisiak, Jacek
Journal of Fluorine Chemistry, 1993 , vol. 60, # 2.3 p. 233 - 237
反应条件
lithium aluminium tetrahydride; titanium tetrachloride; triethylamine in tetrahydrofuran 1.) reflux, 15 min, 2.) r.t., 48 h;
参考文献
Chambers, Richard D.; Roche, Alex J.; Rock, Michael H.
Journal of the Chemical Society. Perkin Transactions 2, 1996 , vol. 1996, # 11 p. 1095 - 1100
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide in N,N-dimethyl-formamide T=70°C;
参考文献
Burton, Donald J.; Yang, Zhen-Yu
Tetrahedron, 1992 , vol. 48, # 2 p. 189 - 275
参考文献
Krespan,C.G. et al.
Journal of the American Chemical Society, 1961 , vol. 83, p. 3428 - 3432
反应条件
sulfur(IV) fluoride; hydrogen fluoride T=170°C; 6 h; Yield given;
参考文献
Dmowski, Wojciech; Porwisiak, Jacek
Journal of Fluorine Chemistry, 1993 , vol. 60, # 2.3 p. 233 - 237
反应条件
sulfur(IV) fluoride T=150°C; 16 h; Yield given. Yields of byproduct given;
参考文献
Dmowski, Wojciech; Porwisiak, Jacek
Journal of Fluorine Chemistry, 1993 , vol. 60, # 2.3 p. 233 - 237
反应条件
sulfur(IV) fluoride; hydrogen fluoride T=130°C; 16 h; Yield given. Yields of byproduct given;
参考文献
Dmowski, Wojciech; Porwisiak, Jacek
Journal of Fluorine Chemistry, 1993 , vol. 60, # 2.3 p. 233 - 237
反应条件
1: sulphur tetrafluoride, hydrogen fluoride / 16 h / 130 °C 2: hydrogen fluoride, sulphur tetrafluoride / 6 h / 170 °C View Scheme
参考文献
Dmowski, Wojciech; Porwisiak, Jacek
Journal of Fluorine Chemistry, 1993 , vol. 60, # 2.3 p. 233 - 237
